development and optimisation of fast, efficient, quantitative, economic and environmentally friendly analytical extraction techniques for the extraction clean up, and pre-concentration in the quantification of 16 usepa priority polycyclic aromatic hydrocarbons (pahs) in contaminated soils have been carried out. three different extraction methods (soxhlet, ultra sonication and mechanical shaking...

ultrasound-assisted extraction was used to determine the optimum processing conditions and to achieve the maximum extraction yield and viscosity of the gum extracted from quince seed. using response surface methodology (rsm) to design the experiments and adopting the central composite rotatable design (ccrd), the effect of extraction temperature (25-55°c), time (3-10 minutes), and ph (6-8) were...

Sample extraction is the first challenge in analysis of herbal medicines (HMs). Numerous methods have been developed to improve extraction efficiency, use less solvent and short time. In this work, a tissue-smashing based ultra-rapid extraction (TSURE) method has been proposed through the designed particle crushing, drastic stir, and dynamic molecular permeation at normal temperature. Factors i...

Ultra thin multilayer capsules are attractive and stable systems capable of delivering the bioactives. Ultra thin multilayer capsules consist of polyelectrolytic materials that are formed in the presence of a template. This is achieved through layer-by-layer adsorption of oppositely charged macromolecules on to colloidal particles. Upon extraction, the resulting cavities retain affi nity for th...

An ultra-fast analytical protocol using graphene-based solid-phase extraction coupled with ultra-performance liquid chromatography-tandem mass spectrometry for the rapid determination of malachite green and its metabolite, leucomalachite green in fish tissues has been developed. In the present work, graphene was synthesized and evaluated as novel solid-phase extraction sorbents for the analytes...

A novel, rapid, simple and sensitive dispersive liquid-liquid microextraction method based on the solidification of floating organic drop (DLLME-SFO) combined with high performance liquid chromatography-ultra violet detection (HPLC-UV) was used to determine acrylamide in potato chips. The derivation of the acrylamide happened in the presence of KBr, KBrO3, H2SO4. Based on studies, 1-undecanol w...

a new approach for a cloud point extraction-electrothermal atomic absorption spectrometric method was used for determining bismuth. the aqueous analyte was acidified with sulfuric acid (ph 3.0–3.5). triton x-114 was added as a surfactant and 2-amino-cyclopentene-1-dithiocarboxylic acid was used as a complexing agent. after phase separation at 50 ◦ c based on the cloud point separation of the mi...