This paper compares the alkali-activated fly ash (AAFA) manufactured with thermal oven curing and pulsed microwave curing methods. Fly ash activated by 8M NaOH solution at a liquid to solid ratio of 0.3 was cured by thermal oven at 85°C and domestic microwave oven, respectively. Apart from compressive strength test, the temperature profiles of AAFA samples were captured by thermal camera. React...

phenolic resins are synthetic low molecular weight thermoset resins which are polymerized and cured to higher molecular weights by condensation method. these resins have high weathering resistance, high oxidative thermal properties and good chemical resistance. phenolic resins can be cured thermally or by acid curing. the most common method of curing phenolic resin is by thermal curing that tak...

Heat generation in an exothermic reaction during the curing process and low thermal conductivity of the epoxy resin produces high peak temperature and temperature gradients which result in internal and residual stresses, especially in large epoxy samples. In this paper, an optimization algorithm was developed and applied to predict the thermal cure cycle to minimize the temperature peak and the...

We commercialized Reactive Coke Agglomerate (RCA), a cement-bonded pellet to decrease the thermal reserve zone temperature for the reduction of the reducing agent rate of blast furnaces. To achieve a high productivity of supplying RCA to large blast furnaces, a rapid curing process of RCA using steam was investigated. We obtained rapid curing of RCA within 18 h by combining primary curing for 1...

A novel trifunctional epoxy resin 4-(3, 3-dihydro-7-hydroxy-2, 4, 4-trimethyl-2H-1-benzopyran-2-yl)-1, 3-benzenediol glycidyl (shorted as TMBPBTH-EPOXY) was synthesized in our lab to improve thermal performance. Its curing behavior and performance were studied by using 4, 4′-diaminodiphenyl sulfone (DDS) as hardener with the mass ratio of 100:41 of TMBPBTH-EPOXY and DDS. The curing activation e...

In order to study the thermal stability of accelerated-curing PF resin, the curing behavior of fresh PF resin was investigated in the presence of single accelerator of methylolurea derivatives (MMU), magnesium hydrate (Mg(OH)2), 25% aqueous solution of sodium carbonate (Na2CO3), and propylene carbonate (PC). Also their optimum combination was added in fresh PF resin. The thermal stability of cu...

one of the common methods to cure unsaturated polyester resins is to use dual initiators. in order to produce an appropriate composite, it is necessary to know the effect of dual initiators on curing behavior. in this paper the effect of benzoyl peroxide, bpo, and tertiary butyl perbenzoate, tbpb, and their mixtures on thermal curing of an unsaturated polyester resin have been investigated. bpo...

This paper reports the characterization of a photosensitive benzocyclobutene (BCB), a low dielectric constant spin-on polymer for use as interlayer dielectric in the microelectronics industry. Research work is divided into three main sections. First, BCB thin film characterization was done to investigate the effects of curing conditions on BCB film thickness, dielectric properties, optical prop...

This paper describes the synthesis and characterization of epoxy resins based on (hexafluoroisopropylidene)diphenol (EFN) and p,p’-isopropylidenebisphenol (EBN), respectively and 4, 4’(hexafluoroisopropylidene)dipthalic-imideamine (IMAM), a curing agent. The synthesized epoxy resins and IMAM curing agent were characterized by Fourier Transform Infrared (FTIR) and 1H Nuclear Magnetic Resonance (...

We synthesized a series of epoxysiloxane oligomers with controllable viscosity and polarity and developed upon them a thermal-curable nanoimprint resist that was cross-linked in air at 110°C within 30 s if preexposed to UV light. The oligomers were designed and synthesized via hydrosilylation of 4-vinyl-cyclohexane-1,2-epoxide with poly(methylhydrosiloxane) with tunable viscosity, polarity, and...