the simulation of distillation columns is an essential step in design, optimization, and rating. in this paper, a new procedure has been proposed for the initial estimation of column profiles based on modified kremser’s group method for simple and/or complex columns. the effect of this initialization algorithm on simulation procedure has been studied through two examples. the results show signi...

  The simulation of distillation columns is an essential step in design, optimization, and rating. In this paper, a new procedure has been proposed for the initial estimation of column profiles based on modified Kremser’s group method for simple and/or complex columns. The effect of this initialization algorithm on simulation procedure has been studied through two examples. The results show sig...

Reactive distillation has received intense attention due to the well known benefits of integrating distillation with reaction in a single unit. While there are procedures available for the synthesis of non-reactive columns and of reaction-separation systems, the design of reactive distillation columns is still a challenge. This work presents a new synthesis and design methodology for reactive d...

A simple experiment such as the batch distillation of an ethanol–water binary mixture can be performed in a 3-h laboratory session using a very rudimentary apparatus consisting of a still pot and two thermocouples. Yet, the results can lead to very interesting insights to distillation and chemical engineering thermodynamics. The present article describes how one can exploit this simple laborato...

The paper discusses distillation column control within the general framework of plantwide control. In addition, it aims at providing simple recommendations to assist the engineer in designing control systems for distillation columns. The standard LV-configuration for level control combined with a fast temperature loop is recommended for most columns.

A5 A PRELIMINARY to the detection and determination of cyanides in biologic materials, a separation by steam distillation is generally employed (1, 2). This may be carried out either in the presence of dilute acid or sodium bicarbonate. It has been stated that the former gives no distinction between the more and the less toxic of the cyanides and that the latter may be unreliable in this respec...

Previously, Tanskanen and Pohjola (2000) and Tanskanen and Malinen (2005) have presented a method of rigorous minimum energy calculation for non-ideal multicomponent distillation. The method is based on column simulation with a large number of equilibrium stages to mimic infinitely high columns, and it has been successfully tested with simple distillation column systems. This paper describes a ...