A chelating resin, cross-linked chitosan modified with the glycine moiety (glycine-type chitosan resin), was developed for the collection and concentration of bismuth in aquatic samples for ICP-MS measurements. The adsorption behavior of bismuth and 55 elements on glycine-type chitosan resin was systematically examined by passing a sample solution containing 56 elements through a mini-column pa...

in this study, cross linked chitosan resin (ccr) was prepared by cross linking chitosan with glutaraldehyde, and then î±-ketoglutaric acid-modified chitosan resin (kcr) was obtained by modifying ccr with î±-ketoglutaric acid. the sorption behavior of methylene blue (mb) on kcr and ccr from aqueous solution was investigated. the effect of various experimental parameters (e.g. initial ph, sorbent...

Catechol-type chitosan resin and salicylic acid-type chitosan resin were easily synthesized for use in estimating the adsorption behavior of 34 elements at pH 1 - 7 in aquatic media. The catechol-type chitosan resin could adsorb Cu(II) at pH 3 - 7, In(III) at pH 4 - 6, Pb(II) and lanthanoids at pH 5 - 7, and U(VI) at pH 4 - 7 more effectively than the salicylic acid-type chitosan resin and the ...

Chitosan was cross-linked using glutaraldehyde in the presence of magnetite. The resin obtained was chemically modified through the reaction with tetraethylenepentamine followed by glycidyl trimethylammonium chlorid to produce chitosan bearing amine (R1) and chitosan bearing both amine and quaternary ammonium chloride moieties (R2), respectively. The quaternary amine resin (R2) showed a higher ...

A novel chitosan-based chelating resin modified with tris(2-aminoethyl)amine moiety (CCTS-TAA) was synthesized, and its characteristics in the collection/concentration of mercury was examined. The synthesized resin showed good adsorption toward mercury in a wide pH range, and the adsorbed mercury can be easily eluted by using 2M HNO(3) without any addition of complexing agent. The resin was the...

A novel L-lysine modified semi-crosslinked chitosan resin (LMCCR) was synthesized and demonstrated to be a promising enzyme support by studying the enzymatic properties of glucose oxidases (GODs) immobilized on it. The prepared LMCCR beads have large specific surface and excellent chemical stability. The insertion of flexible L-lysine spacers between chitosan backbone and the immobilized GODs (...

A sample-pretreatment method using a chitosan-based chelating resin, ethylenediamine-N,N,N'-triacetate-type chitosan (EDTriA-type chitosan), was developed for the preconcentration of trace metals in seawater and separation of the seawater matrix prior to their determination by inductively coupled plasma-mass spectrometry (ICP-MS). The resin showed very good adsorption for transition metals and ...

OBJECTIVES This study evaluated the antibacterial effect and mechanical properties of composite resins (LCR, MCR, HCR) incorporating chitosan with three different molecular weights (L, Low; M, Medium; H, High). MATERIALS AND METHODS Streptococcus (S). mutans 100 mL and each chitosan powder were inoculated in sterilized 10 mL Brain-Heart Infusion (BHI) solution, and was centrifuged for 12 hr. ...

A chitosan resin functionalized with 3-nitro-4-amino benzoic acid moiety (CCTS-NABA resin) was newly synthesized for the collection/concentration of trace molybdenum by using cross-linked chitosan (CCTS) as base material. The carboxyl group of the moiety was chemically attached to amino group of cross-linked chitosan through amide bond formation. The adsorption behavior of molybdenum as well as...

background and purpose: in people wearing dentures, the growth of various candida species under the prosthesis leads to the formation of biofilm, which can play the role of a reservoir for candida and other kinds of microbes. since nano-chitosan particles can cause lasting antimicrobial activity, a more recent approach that utilizes acrylic resins with nano-chitosan particles is proposed. there...