A rapid and efficient method for the synthesis of bis-thiazolidinones has been achieved by pseudo five-component reaction of aldehydes, ethylenediamine and thioglycolic acid in the presence of nano-NiZr4(PO4)6 as catalyst under microwave irradiation. Nano-NiZr4(PO4)6 has been characterized by powder X-ray diffraction, scanning electronic microscopy (SEM), energy dispersive spectroscopy (EDS), v...

A rapid and efficient method for the synthesis of bis-thiazolidinones has been achieved by pseudo five-component reaction of aldehydes, ethylenediamine and thioglycolic acid in the presence of nano-NiZr4(PO4)6 as catalyst under microwave irradiation. Nano-NiZr4(PO4)6 has been characterized by powder X-ray diffraction, scanning electronic microscopy (SEM), energy dispersive spectroscopy (EDS), v...

a novel zinc oxide - agar nanocomposite was successfully synthesized using zinc chloride as a precursor. the nanocomposite was prepared using a domestic microwave oven. the prepared nanocomposites have been characterized by fourier transform infrared (ftir) spectroscopy, x-ray diffraction (xrd) analysis, scanning electron microscopy (sem) and uv- visible spectroscopy. the crystalline properties...

This letter introduces a localized microwave technique for direct excitation of solid materials for the sake of their identification by atomic emission spectroscopy. The microwave energy is concentrated on the material surface by a microwave-drill type applicator. The evolved 1-mm hotspot is slightly evaporated and excited as plasma. An optical spectrometer measures the atomic emission spectrum...

8 1.4.1 Introduction Spectroscopy, or the study of the interaction of light with matter. has become one of the major tools of the natural and physical ciences during this century. As the wavelength of the radiation is varied across the electromagnetic spectrum, characteristic properties of atoms, molecule , liquid and solids are probed. In the optical and ultraviolet regions (A. ""' I J-Lm up t...

The side-arm method for observing chemical recombinations described in the Quarterly Progress Report of April 15, 1958, page 24, is being used to study oxygen-atom recombination within the gas volume and on surfaces. Two modes of volume recombination have been considered: (a) O + 0O3 +0 203 0 03 + O 02 + 02 (b) O + O + 0 2 O + O 2 Reaction (a), involving ozone as an intermediate, proceeds at a ...

in the present study, a simple, efficient and fast synthetic strategy was reported for the green biosynthesis of silver nanostructures (i.e. nanoroads and nanoparticles) by the extract of suaeda acuminata plant, without any catalyst, template or surfactant. aqueous extracts were obtained by maceration and microwave assisted extraction (mae) methods. in mae procedure, the effect of microwave pow...

An efficient and rapid method for the synthesis of 3,4,5-substituted furan-2 (5H)-ones has been achieved through a three-component reaction of aniline, dialkyl acetylenedicarboxylate, and aromatic aldehydes using nano-colloidal silica-tethered polyhedral oligomeric silsesquioxanes with eight branches of 3-aminopropyltriethoxysilane (nano-colloidal silica @APTPOSS) as a superior catalyst under m...