نتایج جستجو برای: microwave promoted synthesis
تعداد نتایج: 503987 فیلتر نتایج به سال:
A phosgene-free synthesis of symmetrical N,N'-disubstituted urea by the reaction of aromatic and aliphatic primary amines and urea promoted by microwave irradiation in the presence of a suitable energy-transfer solvent such as N-N-dimethylacetamide is described.
a phosgene-free synthesis of symmetrical n,n'-disubstituted urea by the reaction of aromatic and aliphatic primary amines and urea promoted by microwave irradiation in the presence of a suitable energy-transfer solvent such as n-n-dimethylacetamide is described.
This paper mainly described the new instruments of microwave-promoted organic synthesis which were appraised, and several microwave-assisted synthetic reactions, such as esterification reaction, orthogonal experimental design and fentanyl synthetic reactions. In comparison with traditional methods of organic synthesis, microwave-assisted chemistry could make high-speed processing of chemical tr...
The application of sequential Ti-/Cu-catalysis in the model one-pot synthesis of benzodiazepine(di)ones promoted by microwave irradiation demonstrates the expediency of dual catalysis in coupling-cyclization methods useful for diversity-oriented synthesis.
[reactions: see text] One-pot total syntheses of the quinazolinobenzodiazepine alkaloids sclerotigenin (1), (+/-)-circumdatin F (2), and (+/-)-asperlicin C (3) via novel microwave-assisted domino reactions were achieved in 55%, 32%, and 20% yields, respectively, from commercially available starting materials. A two-step total synthesis of (+/-)-benzomalvin A (4) was accomplished with an overall...
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