High purity lead titanate nanopowders in tetragonal form have been successfully prepared bycitric acid gel method using lead nitrate and tetra-n-butyl titanate as Pb and Ti sourcesrespectively and citric acid as complexing reagent. The precursors were calcined at varioustemperatures ranging from 450 °C to 600 °C for 2 h. Fourier Transform InfraredSpectroscopy (FT-IR), X-ray diffraction (XRD) an...

high purity lead titanate nanopowders in tetragonal form have been successfully prepared bycitric acid gel method using lead nitrate and tetra-n-butyl titanate as pb and ti sourcesrespectively and citric acid as complexing reagent. the precursors were calcined at varioustemperatures ranging from 450 °c to 600 °c for 2 h. fourier transform infraredspectroscopy (ft-ir), x-ray diffraction (xrd) an...

In this research, the stoichiometric perovskite lead titanate (PbTiO3) nanostructurewas synthesized successfully by the hydrothermal method. The effect of heattreatment of the autoclave and the furnace on the structure of this materialwas investigated. Titanium dioxide (TiO2), titanium tetrachloride (TiCl4) and leadoxide (PbO), lead nitrate (Pb(NO3)2) were used as the ti...

stoichiometric tetragonal bal-xsrxtio3 (x = 0.23) nanopowders were prepared by stearic acid gel(sag) method using barium stearate, strontium stearate, tetrabutyl titanate as ba, sr, ti sourcesand stearic acid as complexing reagent. thermal analysis including differential thermogravimetric(dtg) and tg, fourier transform infrared spectrometry (ftir), x-ray diffraction (xrd) andtransmission electr...

Lead zirconate titanate (PZT) nanopowders with spherical-shaped morphology, perovskite structure and an average size of 20 nm were successfully synthesized. The prepared PZT nanopowders were characterized by differential thermal analysis (DTA), X-ray diffraction (XRD), scanning electron microscopy (SEM), Energy dispersive X-ray (EDS) and Transmission electron microscopy (TEM) technique. Single-...

Stoichiometric tetragonal Bal-xSrxTiO3 (x = 0.23) nanopowders were prepared by stearic acid gel(SAG) method using barium stearate, strontium stearate, tetrabutyl titanate as Ba, Sr, Ti sourcesand stearic acid as complexing reagent. Thermal analysis including differential thermogravimetric(DTG) and TG, Fourier transform infrared spectrometry (FTIR), X-ray diffraction (XRD) andtransmission electr...

Barium-strontium titanate (BST) Ba0.6Sr 0.4 TiO3 and lanthanum-lithium titanate (LLT) La0.5Li0.5TiO3 nanopowders and thin films have been obtained via the modified Pechini route. Polyesterification and complexation processes of gel formation have been examined. Hypothetical models of coordinative polymers formed in sol-gel system have been suggested. It has been shown that BST and LLT solid sol...

nowadays various methods are presented for synthesis of barium strontium titanate (bst) nanopowders with different morphology and properties. each of these (bst)s has got individual characterization that makes it suitable for a special application. every method has a special quality, causes it to have preference over the other methods. low processing temperature is a desired point which most of...

Single-crystalline thin films of complex oxides show a rich variety of functional properties such as ferroelectricity, piezoelectricity, ferro and antiferromagnetism and so on that have the potential for completely new electronic applications. Direct synthesis of such oxides on silicon remains challenging because of the fundamental crystal chemistry and mechanical incompatibility of dissimilar ...