the applicability of hollow fiber-based liquid phase microextraction (hf-lpme) was evaluated for the extraction and preconcentration of loratadine prior to determination by hplc. in order to obtain high extraction recovery, the parameters affecting the hf-lpme including type of organic phase, ph of the source and receiving phases, stirring rate, extraction time and salt addition were studied an...

a simple, inexpensive and efficient method was used for extraction and determination of fexofenadine and levocetirizine with three–phase hollow fiber liquid-phase microextraction and high-performance liquid chromatography. several parameters influencing the extraction recoveries such as the nature of organic extraction solvent, ph of donor and acceptor phases, stirring rate, extraction time and...

an efficient separation-preconcentration procedure namely hollow fiber solid/liquid phase microextraction (hf-slpme) was developed for determination of trace amounts of palladium in water samples by differential pulse voltammetry. in this method, a hybrid sorbent utilizing functionalized nanoparticles incorporated in an organic solvent was used as the extractor phase. the nanoparticle dis­perse...

A simple, inexpensive and sensitive three-phase hollow fiber liquid-phase microextraction (HFLPME) coupled with high performance liquid chromatography (HPLC) with UV detection was successfully developed for determination of trace level of an anti-Histamine drug, fexofenadine, in human plasma and urine. The analyte was extracted into n-octanol that was immobilized in the wall of a porous hollow ...

This work describes a new extraction method with hollow-fiber liquid-phase microextraction based on facilitated pH gradient transport for analyzing hippuric acid and mandelic acid in aqueous samples. The factors affecting the metabolites extraction were optimized as follows: the volume of sample solution was 10 mL with pH 2 containing 0.5 mol·L-1 sodium chloride, liquid membrane containing 1-oc...

this research is on the improvement of the procedure to determination of trace levels of antidepressant drug; fluoxetine in wastewaters. in this research a silica based sol-gel was applied for the extraction of fluoxetine from water samples. this two-phase technique is consisting of aqueous samples of fluoxetine (donor phase) and silica based nanocomposite prepared by sol-gel technique (accepto...

For the first time, hollow-fiber liquid-phase microextraction combined with high-performance liquid chromatography-ultraviolet was used to extract trans,trans-muconic acid, in urine samples of workers who had been exposed to benzene. The parameters affecting the metabolite extraction were optimized as follows: the volume of sample solution was 11 mL with pH 2, liquid membrane containing dihexyl...

In this study a new method of preconcentration, separation and efficient measuring of so-called hollow fiber solid / liquid phase microextraction has been introduced for the determination of trace amounts of lorazepam (LRZ) in water samples, urine and hair using differential pulse voltammetry. To this end, a hybrid adsorbent material was used that involved ionic liquid assisted magnetic multi-w...