abstract our previous studies showed that various extracts of persian shallot (allium hirtifolium) have anti-angiogenic effects. this study has been undertaken to isolate and identify the major effective anti-angiogeneic sub-fraction of shallot. after preparation of the 50% hydroalcoholic extract of shallot bulbs, the extract was successively fractionated into n-hexane, ethyl acetate, n-butanol...

a high performance liquid chromatography method was studied for determination of 18 ?-glycyrrhetinic acid in glycyrrhiza glabra l. (licorice) extract. the operating condition were c-18 reversed phase column (vp-ods, (250×4.6 mm, 5 mm)) at room temperature, acetonitril/phosphoric acid (3/1) as mobile phase, at flow rate of 0.6ml/min (0-8min), 0.4ml/min (8-20min) and uv detection at 230 nm. the r...

a thin-layer chromatography method has been developed and evaluated for the separation and determination of lysine and methonine in a mixture of amino acids obtained from acid or enzyme hydrolysis of protein. the solvent systems were (a) ethanol-ether, (b) phenol-water, (c) ethyl methyl ketone-pyridine-distilled water-glacial acetic acid. procedures in all the three stages were in the same dime...

Determination of sildenafil by various methods and in various media is reviewed in this paper. The methods used consist of ultraviolet (UV) spectroscopy, thin layer chromatography (TLC), and high-performance liquid chromatography (HPLC). These methods were used to determine the amount of sildenafil in pharmaceutical preparations, soft drinks, and biological liquids. HPLC was used for evaluation...

in this assay, the evaluation of lipophilicity of four ace-inhibitors and hydrochlorothiazide (hctz) with rp-tlc on cellulose layers was described using three binary solvent systems. the selected ace inhibitors had sufficiently different structures which can indicate the method suitability for their lipophilicity evaluation as the model substances in comparison with hctz. in addition, the linea...

objective: during recent years, opium consumption has increased among iranian diabetic men. the belief that opium consumption can control or even eradicate dm is increasing. this study was conducted to compare the blood sugar, hba1c, lipid profile and the frequency of diabetes complications in male type ii diabetic patient with and without opium consumption. materials and methods: two hundred t...

aims: the synthetic colors are preferred by the food industry because of the variety of shades, intensity, uniformity, excellent solubility and stability. they are used in a variety of food products such as dairy products, beverages, baked products, confections and pet foods. food colors may have toxic effects on the human body. this study aimed to examine the amount of synthetic colors in some...

stachys genus with medicinal properties and high polymorphic features has been considered oneof the largest genera of lamiaceae. the aim of this study was to determine the flavonoid patternvariations and flavonoid groups in ten stachys species belonging to two sections; fragilicaulis,and aucheriana. the studied species were collected from natural habitats in iran and analysedfor their flavonoid...