نتایج جستجو برای: headspace solid phase microextraction

تعداد نتایج: 755834  

Journal: :مجله دانشگاه علوم پزشکی قم 0
حمیدرضا حیدری hr heidari qom university of medical sciencesدانشگاه علوم پزشکی قم سید جمال الدین شاه طاهری sj shahtaheri tehran university of medical sciencesدانشگاه علوم پزشکی تهران محمود علیمحمدی m alimohammadi tehran university of medical sciencesدانشگاه علوم پزشکی تهران عباس رحیمی فروشانی a rahimi-froshani tehran university of medical sciencesدانشگاه علوم پزشکی تهران فریده گلبابایی f golbabaei tehran university of medical sciencesدانشگاه علوم پزشکی تهران

background and objectives: analytical methods for volatile organic compounds (vocs) in different samples need extraction of compounds, by applying hazardous solvents. solid phase micro-extraction (spme) is a solvent-free equilibrium extraction method, in which proper calibration can allow quantitative determinations of vocs at a very good sensitivity without the use of any organic solvent. vocs...

Journal: :iranian journal of public health 0
hr heidari dept. of occupational health sj shahtaheri dept. of occupational health, center for environmental research m alimohammadi dept .of environmental health a rahimi-froshani dept. of epidemiology and biostatistics, school of public health, tehran university of medical scien

background: determination of organic pollutants usually requires extraction of the pollutants from samples, using hazard­ous solvent. solid phase micro-extraction (spme) is a solvent-free equilibrium extraction method, in which, proper calibra­tion can allow quantitative measurements of organic pollutants at a very good sensitivity without the use of any organic sol­vent. because individual voc...

Journal: :research journal of pharmacognosy 2014
s. saeidnia z. sepehrizadeh a.r. gohari g. amin a. manayi

dracocephalum kotschyi (lamiaceae), as one of the remarkable aromatic plants, widely grows and also is cultivated in various temperate regions of iran. there are diverse reports about the composition of the oil of this plant representing limonene derivatives as its major compounds. there is no report on cloning of mono- or sesquiterpene synthases from this plant. in the present study, the aroma...

Journal: :iranian journal of chemistry and chemical engineering (ijcce) 2014
mansoor anbia morteza khazaei

in this paper, the possibility of using a new ordered nanoporous carbon as a new fiber in headspace solid phase microextraction (hs-spme) to determine of mononitrotoluenes (mnts) in waste water is demonstrated. the structural order and textural properties of the ordered nanoporous carbon were studied by x ray diffraction (xrd), scanning electron microscopy (sem) images and nitrogen adsorption i...

2004
Derrick C. Wood James M. Miller

2 Headspace sampling for gas chromatographic (GC) analysis has many advantages, the most important of which is the elimination of many interferences from the sample matrix. In addition to the standard methods for headspace sampling, the technique of solid-phase microextraction (SPME) has found wide acceptance because it is simple and inexpensive. More recently, single-drop microextraction (SDME...

2000

Compound-specific carbon isotope ratio analysis is a promising tool to assess the origin and fate of organic contaminants in groundwater. The aim of this study was to develop and evaluate a reliable, fast method to determine carbon isotope ratios of chlorinated methanes, ethanes, and ethenes in aqueous samples. Direct solid-phase microextraction (dSPME) and headspace solid-phase microextraction...

Journal: :caspian journal of chemistry 2014
mohammad h fatemi hanieh malekzadeh alireza ghassempour vahide mahdavi

a combined gas chromatography–mass spectrometry (gc–ms) with headspace solid-phase microextraction (hs-spme) method has been employed for the analysis of the flavor volatiles of some iranian rice cultivars (domsiah, deylamani, hashemi, shirodi and tarom). the samples were grown in different cities of mazandaran province. the sampling procedure and chromatographic conditions were same for all sa...

2014
Murat Yilmaztekin

Volatile components in cape gooseberry fruit at ripe stage were collected using headspace-solid phase microextraction, and analyzed by gas chromatography-mass spectrometry. Three solid phase microextraction fiber coatings (DVB/CAR/PDMS, CAR/PDMS, and PDMS/DVB) were tested for evaluation of volatile compounds. DVB/CAR/PDMS fiber showed a strong extraction capacity for volatile compounds and prod...

2007
Dragana Mutavdžić Pavlović Sandra Babić Alka J.M. Horvat Marija Kaštelan-Macan

Abbreviations: AIBN, 2,20-azo-bis-isobutyronitrile; ASE, Accelerated solvent extraction; CAR, Carboxen; DAD, Diode-array detector; DI-SPME, Direct-immersion solid-phase extraction; DSPE, Dispersive solid-phase extraction; EGDMA, Ethylene glycol dimethacrylate; ESE, Enhanced solvent extraction; ESI, Electrospray ionization; FD, Fluorescence detection; FLD, Fluorimetric detection; GC, Gas chromat...

Journal: :Zeitschrift fur Naturforschung. C, Journal of biosciences 2001
F Demirci N Kirimer B Demirci Y Noma K H Başer

In the course of our continuing work on transformation of monoterpenes by microorganisms, the biotransformation of (+)- and (-)-carvone was carried out. The metabolites formed during microbial transformations were screened using a simple, rapid and efficient technique: Headspace-solid phase microextraction (SPME)/GC-MS. The results as well as the application of this technique are described.

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