the cunica nanopanicles have been synthesized by sol-gel auto-combusson. microwave and co-precipitationtechniques. then, the results of the three techniques were compared. in the vol-ael auto-combustion synthesiswas used glycine as a fuel. at first, sol was prepared. then, gel was achieved from drying so'. the prepared gelwas burnt at 350°c. in the noicrowavc technique, gel was prepared. then, ...

in this paper, indium tin oxide (ito) nanoparticles has been prepared by chemical methods under given conditions with solution of indium chloride (incl3·4h2o), tin chloride (sncl4·5h2o) in ammonia solution. the samples were characterized by x-ray diffraction (xrd) and scanning electron microscopy (sem) analyses after heat treatments. the sem results showed that, the size of the ito particles pr...

in this study, sio2 nanoparticles were successfully synthesized via sol-gel precipitation method and the effects of different parameters such as temperature, ethanol, ammonia and tetraethylorthosilicate (teos) contents based on water were investigated in a systematic way applying taguchi experimental design method. it was found that, among all the investigated parameters, ethanol as a co-solven...

Urea amidolyase was purified to homogeneity from extracts of Candida utilis. The purification involves protamine sulfate precipitation, ammonium sulfate precipitation, polyethylene glycol precipitation, Sepharose 6B gel filtration, DEAE-cellulose column chromatography, and hydroxylapatite column chromatography. The final preparation is pure as judged by disc-gel electrophoresis. The molecular w...

Controlling and engineering chemical structures are the most important scientific challenges in material science. Precipitation patterns from ions or nanoparticles are promising candidates for designing bulk structure for catalysis, energy production, storage, and electronics. There are only a few procedures and techniques to control precipitation (Liesegang) patterns in gel media (e.g., using ...

background: detecting bence-jones protein in urine is essential for determining plasma cell dyscrasia and multiple myeloma. conventionally, acid-heat precipitation assay is used for detecting bence-jones protein in most medical laboratories; however, because of the low accuracy of this test, other more sensitive tests like urine electrophoresis are recommended.  materials and methods: in this s...

INTRODUCTION The aim of the study was to evaluate two methods of macroprolactin (MaPRL) detection - precipitation with polyethylene glycol (PEG) and ultrafiltration and to compare these techniques with "gold standard" - gel filtration chromatography (GFC). MATERIAL AND METHODS The study was conducted on 245 patients - 45 with organic and 200 with functional hyperprolactinaemia. In all the sub...

The mechanisms responsible for spontaneous silver precipitation in silver-doped sol-gel materials are identified. The chemistry of the solvent phase is found to be the critical factor in controlling this phenomenon. The addition of HCl as catalyst leads to the formation of AgCl and subsequent formation of silver upon light exposure. Another factor leading to silver precipitation is the reducing...

The mechanisms responsible for spontaneous silver precipitation in silver-doped sol-gel materials are identified. The chemistry of the solvent phase is found to be the critical factor in controlling this phenomenon. The addition of HCl as catalyst leads to the formation of AgCl and subsequent formation of silver upon light exposure. Another factor leading to silver precipitation is the reducing...