a simple, highly sensitive, accurate and selective method was presented for determination of trace amounts of cu (ii) in water samples. the stability of an n, n´ -disalicylideneethylenediamine modified nano geraphene especially in concentrated hydrochloric acid was studied which used as a recycling and pre-concentration reagent for further uses of n, n´-disalicylideneethylenediamine modified na...

N(2-Thiophenyl)-1-(2-hydoxyphenyl)Imine (NTPHPI) was used as a proper complexing agent for the preconcentration by cloud point extraction followed by atomic absorption spectrometric to determine of Ni, Cu and Co ions in real samples. NTPHPI and Triton X-114 were used as hydrophobic ligand and non-ionic surfactant respectively and the pH of 8 was chosen as optimum. Under the optimized experiment...

A simple, highly sensitive, accurate and selective method for determination of trace amounts of Cu2+ in water samples was reported. In this paper, Isopropyl 2-[(isopropoxy carbothioyl)disulfanyl]ethanethioate (IIDE) in order to prepare an effective sorbent for the preconcentration and determination of Cu. The sorption capacity of Isopropyl 2-[(isopropoxy carbothioyl)disulfanyl]ethanethioate (II...

a simple, highly sensitive, accurate and selective method for determination of trace amounts of cu2+ in water samples was reported. in this paper, isopropyl 2-[(isopropoxy carbothioyl)disulfanyl]ethanethioate (iide) in order to prepare an effective sorbent for the preconcentration and determination of cu. the sorption capacity of isopropyl 2-[(isopropoxy carbothioyl)disulfanyl]ethanethioate (ii...

A simple, highly sensitive, accurate and selective method for determination of trace amounts of Cu2+ in water samples was reported. In this paper, Isopropyl 2-[(isopropoxy carbothioyl)disulfanyl]ethanethioate (IIDE) in order to prepare an effective sorbent for the preconcentration and determination of Cu. The sorption capacity of Isopropyl 2-[(isopropoxy carbothioyl)disulfanyl]ethanethioate (II...

A rapid separation and preconcentration method was developed for the determination of trace metals Cu, Zn, Cd, and Pb in seawater using a minicolumn packed with thiol cotton fiber (TCF) coupled with inductively coupled plasma mass spectrometry (ICP-MS). Preconcentration parameters, such as seawater sample volume and flow rate and eluent hydrochloric acid concentration, volume and flow rate, wer...

In this study, the potential of 8-Hydroxyquinoline grafted SBA-15 to extract of Cu2+ cations from aqueous solutions was investigated. SBA-15 nanoporous silica was chemically grafted with 8-Hydroxyquinoline groupsaccording to the procedure in the literature. The presence of organic groups in the silica framework was demonstrated by FTIR spectrum. The grafted product showed th...

the aim of this work was to develop a new and simple coacervative extraction method for the preconcentration and spectrophotometric determination of cu(ii) in water samples. dithizone was used as the chelating agent while an anionic surfactant, namely sodium dodecyl sulfate (sds), was used as extracting agent at room temperature. central composite design (ccd) based on response surface methodol...

In this project by the use of cilicagel as Sorbent for preconcentration of traces of Cu and Zn considered by Solid Phase Extraction prior to determination by flame Atomic Absorption Spectroscopy (FAAS). In this method 4,2 Pyridilazo resorsinol (PAR) as a complexing agent For copper and zinc ion after adsorbed in cilicagel and after that eluted by 5 ml of nitric Acid (3M). Some effective Paramet...

A versatile preconcentration system for trace element determination by ICPMS was developed. It is composed of a commercial flow injection analysis system (FIAS) retrofitted with a home-made control unit containing three solenoid valves and working concomitantly with the FIAS, permitting selection and segmentation of sample, reagent, washing solution and elution flow. The knotted reactor used ha...