Nanostructured Cu-20Fe alloy was synthesized by mechanical alloying process and the effects of process control agents (PCA) on the phase formation, crystallite refinement and morphology of powder particles were studied. The dissolution of Fe into Cu matrix and the morphology of powder particles were analyzed by X-ray diffraction (XRD) technique and scanning electron microscopy (SEM), respective...

The structural evolution of nanocrystalline TiO2 was studied by X-ray diffraction (XRD) and the Rietveld refinement method (RRM). TiO2 powders were prepared by the sol-gel technique. Post annealing of as-synthesized powders in the temperature range from 500 degrees C to 800 degrees C under air and argon atmospheres led to the formation of TiO2 nanoparticles with mean crystallite size in the ran...

The effects of plastic deformation by ball milling on the structure of a partly amorphousAl87Ni8La5alloy were investigated by X-ray diffractometry. Lattice parameter, crystallite size and lattice strain of the fcc-Al precipitates were determined by Rietveld refinement, doubleVoigt approach and Williamson-Hall plots. The changes in lattice parameter of fcc-Al nanoprecipitates during ball milling...

The particle size distribution of the resultant cobalt ferrite samples was determined from Scanning Electron Microscopy (SEM) images using the granulometry image analysis method. Results showed the nanosized particles of the samples. The X-Ray Diffraction (XRD) patterns of samples were also analyzed by Rietveld refinement method. The results indicated that the precipitated sample at 95 <sup...

The microstructure of gold catalysts supported on rutile was obtained by Rietveld refinement. Three-dimensional images of the crystallites were generated in real space, as well as 3-D images of the microstrain distribution in reciprocal space. These images were used to analyze the effect of the different parameters of the refinement models on the interpretation of the microstructure of the samp...

Equal channel angular rolling (ECAR) is a severe  plastic deformation (SPD) technique which has been used to produce metal sheets with ultra-fine grain structure. In the present work, the relationships between the mechanical properties and microstructure of samples during the ECAR process have been investigated. The Rietveld method was applied to analyze the X-ray diffraction pattern and to det...

Fe-Mn-C austenitic steels exhibit outstanding high-ductile deformation in their plastic regions along with significant microstructural evolution. In this study, to characterize the microstructural evolution during deformation of these steels, line-profile and texture analyses were carried out using X-ray diffraction. The convolutional multiple whole profile fitting procedure was used for a line...

TiO2 nanoparticles with attractive physicochemical properties have synthesized by means of the sol-gel method and acid hydrolysis. The obtained nanoparticles have characterized by the XRD-Rietveld refinement, BET and TEM techniques, and tested in the photodecomposition of acetaldehyde. The degree of decomposition of acetaldehyde by the sol-gel TiO2 nanoparticles was directly proportional to the...