in this scientific research work we report a novel method to synthesis co3o4 nanoparticles via calcinations of cobalt hydroxide which can be conveniently prepared by the co(no3 )2.6h2o with different reactants. in order to study the effect of calcination temperature on structure and morphology of the nanoparticles, the calcinations take place at various temperatures (at 300°c, 500°c and 700°c)....

A facile thermal-treatment route was successfully used to synthesize ZnO nanosheets. Morphological, structural, and optical properties of obtained nanoparticles at different calcination temperatures were studied using various techniques. The FTIR, XRD, EDX, SEM and TEM images confirmed the formation of ZnO nanosheets through calcination in the temperature between 500 to 650 °C. The SEM images s...

The kinetics of calcination of a high calcium type of limestone was studied. Ukpilla limestone found in the central region of Nigeria was studied. The limestone composition shows that the limestone has 51.29% calcium oxide and 41.53% loss on ignition and magnesium oxide content of 2.23%. The following parameters were determined; diffusion coefficient of lime layer, and mass transfer coefficient...

Yttrium iron garnet powders have been synthesized by chemical coprecipitation using two different precursors, nitrates and chlorides, and by an oxides mixture route. It is shown that depending on the precursors and synthesis conditions used pure yttrium iron garnet powders can be obtained with a mono or multidomain magnetic behaviour. The yttrium iron garnet crystalline structure, as studied by...

In this paper, mesoporous alumina with different pore sizes and wall crystalline structures was synthesized at calcination temperatures over 550 degrees C. The characterization of the samples calcined at 550, 800, 1100, and 1300 degrees C, respectively, was performed using TEM, XRD, FTIR, TG/DTA, and N2 adsorption/desorption techniques. The correlation between pore size and wall crystalline str...

The calcination reaction of limestone (CaCO3) to yield lime (CaO) is at the heart of many industrial applications as well as natural processes. In the recently emerged calcium-looping technology, CO2 capture is accomplished by the carbonation of CaO in a gas-solid reactor (carbonator). CaO is derived by the calcination of limestone in a calciner reactor under necessarily high CO2 partial pressu...

−A study of the phase transformations generated by chlorine during the calcination of clays and kaolins is presented. The original samples and residues of the thermal treatment carried out in air and chlorine atmospheres are analyzed at different calcination times and temperatures. Sample characterization was performed by X-ray diffraction (XRD), scanning electron microscopy (SEM) and Xray micr...

in this work, hydrochloric acid is used to remove iron impurities in the bauxite ore contained in the diasporite mineral located in the sari region. the bauxite ore was calcined at different temperatures and times, and then dissolved in a hydrochloric acid solution. after determining the optimum calcination conditions in 1 h at 900 °c, the response surface methodology (rsm) with four factors in...

In this study, an effective low-temperature method was developed, for the first time, for the synthesis of bismuth titanate nanobelts by using Na2Ti3O7 nanobelts as the reactants and templates. The experimental procedure was based on ion substitution followed by a nanoscale solid-state reaction. In the first step, Na2Ti3O7 nanobelts were soaked in a bismuth nitrate solution where ion substituti...

The conversion of thermally pretreated CaO along successive carbonation/calcination cycles has been investigated, as a ected by looping-calcination conditions, by means of Thermogravimetric Analysis (TGA). Sorbent samples have been subjected in-situ to a thermal preheating program based on Constant Rate Thermal Analysis (CRTA) by virtue of which decarbonation is carried out at a low controlled ...