An efficient and green protocol for the synthesis of αaminonitriles derivatives by one-pot reaction of different aldehydes with amines and trimethylsilyl cyanides has been developed using natural alumina, alumina sulfuric acid (ASA), nano-γ-alumina, nanoalumina sulfuric acid (nano-ASA) under microwave irradiation and solvent-free conditions. The advantages of methods are short reaction times, h...

The Fe nanowires were prepared by Ac electrodeposition method. The two steps anodized aluminum oxides (alumina) were used as templates for electrodeposition of magnetic nanowires. Sulfuric acid was used to anodize aluminum. The pours diameter and growth rate of alumina were investigated. The FeSO4 electrolyte was used for growth of nanowires. The prepared magnetic nanowires were characterized b...

In this study, the recovery of platinum and palladium from petroleum catalysts has been elaborated using a method consisting mainly of dissolving alumina substrate in sulfuric acid thereby concentrating the precious metals in the residue. The effect of dissolution temperature and time, concentration of sulfuric acid, and pulp density on the dissolution of alumina substrate was investigated syst...

a novel and safe method for nitration of phenols, anilines and other aromatic compounds has beenfound to be feasible with alumina sulfuric acid (asa) as catalyst and mg (no3)2.6h2o as nitrating agent inneat water as solvent. the use of water makes this method compatible with the green chemistry approach

The electron capture gas liquid chromatography test method for chick edema factor has been modified by replacing the alumina column s t ep with an additional sulfuric acid cleanup and a caustic wash which permits a reduction in sample cleanup time. Samples are subjected to double preliminary sulfuric acid cleanup and caustic wash and extracted each time with t r imethyl pentane. The final extra...

The urinary metabolites of N-2-fluorenylacetamide were separated by chromatography on an alumina column into three classes: (a) unconjugated materials, amounting to 5-10 per cent of the urinary activity; (b) sulfuric acid conjugates (20-25 per cent); (c) glucuronic acid conjugates (60-70 per cent). Evidence for the structure of these materials was adduced by solvent partition, paper chromatogra...

in this work, a tracer study on pore initiation in anodic alumina in oxalic acid was performed. effects of some experimental parameters such as applied electrical potential, electrolyte composition and heat pretreatment were evaluated. electrochemical and morphological experiments were performed using potentiostatic anodizing and scanning electron microscopy (sem) techniques, respectively. effe...

A continuous process for the preparation of structurally well-defined uniform alumina (Al2O3) nanotubes was developed. The present nanofabrication approach is based on pulse anodization of aluminum by using sulfuric acid and provides unique opportunity for a facile tailoring of the length of nanotubes by controlling the pulse duration.

In this work, a tracer study on pore initiation in anodic alumina in oxalic acid was performed. Effects of some experimental parameters such as applied electrical potential, electrolyte composition and heat pretreatment were evaluated. Electrochemical and morphological experiments were performed using potentiostatic anodizing and scanning electron microscopy (SEM) techniques, respectively. Effe...