nano silica-h2so4 is an efficient and mild catalysis system for the regeneration of aldehyde from aldoximes. ketoximes are converted to amides by beckmann rearrangement in the presence of nano silica-h2so4. the reactions are carried out in solvent-free conditions under microwave irradiation (600 w) within 50-120 sec in good yields.

polyamide-66(pa66)/caco3 micro- and nano-composites were prepared using a polymer solution method at filler loading of 0, 1, 2 and 3 weight percent. nano-size of caco3 was synthesized by micro-emulsion technique. the material was characterized by xrd, sem, ftir and uv-vis techniques. xrd results of composites suggested that caco3 particles are found in the amorphous phase of the semi-crystallin...

a new simple and reliable method for rapid and selective extraction and determination of trace levels of zn(ii) ion is developed. zn(ii) ions are adsorbed quantitatively during passage of aqueous samples through pet-aa/aam nano fiber modified. almost all matrix elements were found to pass through the nano fiber to drain. modified poly (ethylene terephthalate)-grafted-acrylic acid/acryl amide na...

Encapsulation of a cationic carbodiimide condensing agent within a self-assembled hexameric capsule made of resorcin[4]arene units provides a nano-environment that efficiently steers the substrate selectivity in the amide synthesis reaction between carboxylic acids and primary amines. While in solution pairs of acids react similarly with a given amine, in the presence of the capsule the formati...

in this paper functionalized multiwall carbon nanotubes (fmwcnt) were modified using doxycycline, containing reactable nitrogen, which can attach chemically to functionalized mwcnt. the synthesized nano compounds were characterized by fourier transform infrared spectroscopy (ft-ir) and raman spectroscopy. these spectrums proved the existence of nitrogen atoms of amide functional groups. the mor...

Polyamide-66(PA66)/CaCO3 micro- and nano-composites were prepared using a polymer solution method at filler loading of 0, 1, 2 and 3 weight percent. Nano-size of CaCO3 was synthesized by micro-emulsion technique. The material was characterized by XRD, SEM, FTIR and UV-VIS techniques. XRD results of composites suggested that CaCO3 particles are found in the amorphous phase of the semi-crystallin...

In this paper functionalized multiwall carbon nanotubes (FMWCNT) were modified using doxycycline, containing reactable nitrogen, which can attach chemically to functionalized MWCNT. The synthesized nano compounds were characterized by Fourier transform infrared spectroscopy (FT-IR) and Raman spectroscopy. These spectrums proved the existence of nitrogen atoms of amide functional groups. The mor...

ÐDevelopments in the ®eld of magnetic materials which show promise for future applications are reviewed. In particular recent work in nanocrystalline materials is reviewed, with either soft or hard behavior as well as advances in the magnetic materials used for magnetic recording. The role of microstructure on the extrinsic magnetic properties of the materials is stressed and it is emphasized h...

* Corresponding Author Email: [email protected] Objective(s): The main aim of current research was to develop a novel magnetically responsive hydrogel by radical polymerization of carboxymethyl cellulose (CMC) on acryl amide (Am) using N,N'-methylene bis acrylamide (MBA) as a crosslinking agent, potassium persulfate (KPS) as a free radical initiator, and magnetic montmorillonite ( mMT)...

In this paper functionalized multiwall carbon nanotubes (FMWCNT) were modified using doxycycline, containing reactable nitrogen, which can attach chemically to functionalized MWCNT. The synthesized nano compounds were characterized by Fourier transform infrared spectroscopy (FT-IR) and Raman spectroscopy. These spectrums proved the existence of nitrogen atoms of amide functional groups. The mor...