يتضمن البحث تحضَير عدد من مشتقات6-bromo-2-phenylquinoline-4-carboxylic acid ، وقد تم تشخيصها بوساطة قياس درجة الانصهار والتحليل الكمي الدقيق للعناصر (C.H.N.S) وطيف الرنين النووي المغناطيسي للبروتون (1H-NMR) و تحليل طيف الأشعة تحت الحمراء (FT-IR) . ومن المركبات المحضرة
 1-تحضير المركب [A1] 6-bromo-2-phenylquinoline-4-carboxylic acid
 2-تحضير 6-bromo-2-phenylquinoline-4-carboxyl chloride...

Reaction of methyl 3-bromo-5-cyanoisothiazole-4-carboxylate with conc. H2SO4 gave 3-bromo-5-carbamoylisothiazole-4-carboxylate in 93% yield. The compound was fully characterized.

In this paper, we report on the crystal structure of salt 1-(4-bromo-2,3,5,6-tetrafluorophenyl)-3-(3-phenylbenzyl)-4-methylimidazolium bromide, 3, synthesized by sequential nucleophilic attack 4-methylimidazole bromopentafluorobenzene and then 3-phenylbenzyl bromide. The was characterized 1H, 13C, 19F NMR spectroscopy mass spectrometry.

In the title compound, C(7)H(9)BrN(+)·ClO(4) (-), the cations and anions are linked by inter-molecular N-H⋯O hydrogen bonds, forming a two-dimensional network parallel to the ab plane.

In the title compound, C(8)H(7)BrO(3), the meth-oxy-carbonyl group is twisted at a dihedral angle of 8.06 (4)° with respect to the benzene ring. In the crystal, mol-ecules are connected by O-H⋯O hydrogen bonds into helical chains running along the b axis.