Poly(3-hexylthiophene) (P3HT) nanoparticles (NPs) were prepared by a reprecipitation method. Hydrothermal processing applied external pressure to the pristine P3HT NPs at temperatures ranging from 60 to 150 °C. Optical absorption and photoluminescence (PL) spectra for the hydrothermally treated P3HT NPs varied markedly with the processing temperature. With increasing treatment temperature, the ...

Silver (Ag) nanoparticle-loaded strontium titanate (SrTiO₃) nanoparticles were attempted to be synthesized by a sol-gel-hydrothermal method. We prepared the titanium oxide precursor gels incorporated with Ag⁺ and Sr2+ ions with various molar ratios, and they were successfully converted into the Ag-SrTiO₃ hybrid nanoparticles by the hydrothermal treatment at 230 °C in strontium hydroxide aqueous...

A novel hydrothermal zirconium oxide (ZrO2) ion exchange material was successfully synthesized by hydrothermal technique. The material has been characterized using different tools such as thermal analysis (DTA-TGA), FT-IR and X-ray diffraction studies. The results show that the prepared ZrO2 is pure and with a unique shape and it belongs to the hexagonal system. Chemical resistively of the mate...

Gapped hollow BaTiO3 nanospheres with an apparent diameter of 93 ± 19 nm (shell thickness of 10-20 nm) were synthesized via a dynamic hydrothermal process using TiO2 sols and Ba(2+) ions as the Ti and Ba sources in alkaline aqueous solutions. The phases and morphologies of the BaTiO3 samples were characterized by X-ray diffraction (XRD), SEM, TEM, and Raman spectra. The effects of the hydrother...

Effect of hydrothermal treatment, acid washing and annealing temperature on the structure and morphology of TiO2 nanotubes during the formation process was assessed. X-ray diffraction, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and energy dispersive X-ray spectroscopy analysis were conducted to describe the formation and characterization of the structure and morp...

The mechanical and physical properties of composite materials are greatly influenced by the structure and properties of fiber/matrix interface. Short beam shear test is often performed to evaluate the laminar interface properties in real applications, especially for studying them after a given hydrothermal treatment. However, the results depend on the interface and the matrix properties, so the...

Rod-like hydroxyapatite nanoparticles (n-HAp) with a highly ordered nanostructure were prepared by hydrothermal synthesis from calcium chloride, and phosphoric acid, as calcium and phosphorus sources, respectively. Various surfactant families such as cationic (CTAB), anionic (SDS) and nonionic (Triton X-100) were used as regulators of the nucleation and crystal growth. The synthesized nanopowde...

Silica gel was prepared and treated thermally and hydrothermally and was characterized as solid stationary phase in gas chromatography. The characteristics have been evaluated in terms of polarity, selectivity, and separation efficiencies. These parameters were used to assess the outer silica surface contributions and the degree of surface deactivation brought about by different treatment techn...

in this research work, it was planned to study influences of hydrothermal treatment temperature, holding time and press temperature on wood density, spring back, moisture absorption as well as dimensional stability of combined-hydro-thermo-mechanically modified poplar wood. wood blocks were treated hydrothermally at temperatures 120, 150 and 180°c for holding time of 0, 30 and 90 min. afterward...

this study was carried out to determine the effect of fermentation, hydrothermal treatment, soda (na2co3), and table salt (nacl) addition on the extent of phytase activity and phytate degradation in three iranian wheat cultivars, namely, mahdavi, ghods, and roshan. the samples were milled to three different extraction rates, i.e. whole, 85%, and 75% flours and three kinds of leavening procedure...