The freeze-etching technique must be improved if structures at the molecular size level are to be seen. The limitations of the technique are discussed here together with the progress made in alleviating them. The vitrification of living specimens is limited by the fact that very high freezing rates are needed. The critical freezing rate can be lowered on the one hand by the introduction of anti...

The freeze-etching technique must be improved if structures at the molecular size level are to be seen. The limitations of the technique are discussed here together with the progress made in alleviating them. The vitrification of living specimens is limited by the fact that very high freezing rates are needed. The critical freezing rate can be lowered on the one hand by the introduction of anti...

the liquid metal flow and the solidification behaviours in a multi-cavity casting mould of two automotive cast parts were simulated in three dimensions. the commercial code, flow-3d® was used because it can track the front of the molten metal by a volume of fluid (vof) method and allows complicated parts to be modeled by the fractional area/volume obstacle representation (favor) method. the gre...

Freeze casting for Al2O3 was accomplished at room temperature with nonaqueous sublimable vehicles in the naphthalene– camphor eutectic system with a eutectic temperature of 31°C. A fully dense sintered body (>99.5% of theoretical density (T.D.)) was obtained with a eutectic composition vehicle, whereas at most 90% T.D. was obtained with an off-eutectic (i.e., hypoor hypereutectic) composition v...

Freestanding electrodes are a promising way to increase the energy density of batteries by decreasing overall amount electrochemically inactive materials. antimony doped tin oxide (ATO)-based hybrid materials have not been reported so far, although this material has demonstrated excellent performance in conventionally designed electrodes. Two different strategies, namely electrospinning and fre...

INTRODUCTION Innovative metal/ceramic composites produced by melt infiltration of innovative ceramic preforms prepared by a freeze casting technique are examined in this study. These composites exhibit a characteristic hierarchical structure: On a mesoscopic length scale, lamellar domains with sizes up to several millimetres are observed (Fig. 1). The aim of the present study is to analyze the ...