A calcium sennoside was extracted by developed microwave assisted extraction technique from Senna leaves. Microwave extraction was carried out at 250 W for 20 minutes, 350 W for 15 minutes and 450 W for 10 min heating period, these produced increase yields of calcium sennosides when compared to conventional heating. The yield of calcium sennosides obtained by microwave extraction was found to b...

Combination of the surfactant-free nonaqueous sol–gel approach with the microwave technique makes it possible to synthesize Fe3O4, CoFe2O4, MnFe2O4, and NiFe2O4 nanoparticles of about 5–6 nm and with high crystallinity and good morphological uniformity. The synthesis involves the reaction of metal acetates or acetylacetonates as precursors with benzyl alcohol at 170 C under microwave irradiatio...

background & aim: a simple and rapid microwave- assisted extraction (mae) procedure was developed and optimized for the isolation of borneol and bornyl acetate from ferulago macrocarpa. ferulago macrocarpa (apiaceae) is an endemic plant in iran. experimental: dried powdered aerial parts of plants were soaked in water and irradiated with microwave in a clevenger extraction approach under opt...

GdCaAl3O7:Eu red nano-phosphors were synthesized by solution combustion using urea as fuel. Fourier-transform infrared, X-ray diffraction, scanning electron microscope, transmission electron microscope and photoluminescence spectrophotometer were used to characterize the obtained samples. XRD patterns revealed that GdCaAl3O7:Eu pure phase was formed by combustion of metal nitrate solution in th...

Ionic liquid based, microwave-assisted extraction (ILMAE) was successfully applied to the extraction of proanthocyanidins from Larix gmelini bark. In this work, in order to evaluate the performance of ionic liquids in the microwave-assisted extraction process, a series of 1-alkyl-3-methylimidazolium ionic liquids with different cations and anions were evaluated for extraction yield, and 1-butyl...

Coupling with robust surfaces is a promising approach to improve the stability and recyclability of highly active molecular catalysts. This study builds on our prior success to deposit a Co(iii) cyclam complex, where cyclam is 1,4,8,11-tetraazacyclotetradecane, on mesoporous silica via a microwave-assisted process. The Co(iii) complex was successfully deposited on the silica surface through rea...

An ultrasound and microwave assisted alternant extraction method (UMAE) was applied for extracting dihydroquercetin (DHQ) from Larix gmelinii wood. This investigation was conducted using 60% ethanol as solvent, 1:12 solid to liquid ratio, and 3 h soaking time. The optimum treatment time was ultrasound 40 min, microwave 20 min, respectively, and the extraction was performed once. Under the optim...

In this study, extraction of essential oil, polyphenols and pectin from orange peel has been optimized using microwave and ultrasound technology without adding any solvent but only "in situ" water which was recycled and used as solvent. The essential oil extraction performed by Microwave Hydrodiffusion and Gravity (MHG) was optimized and compared to steam distillation extraction (SD). No signif...

Microwave-assisted dilute acid/alkali pretreatment is an efficient and rapid method of removing lignin and hemicellulose, however, the optimized parameters for the maximum efficiency have to date not been presented in the literature. The purpose of this study was to determine those conditions by examining the effects of three factors: microwave power, temperature, and time on delignification in...

A new kind of silver indium tungsten oxide (AgIn(WO(4))(2)) mesocrystals with high hierarchy can be synthesized by a microwave-assisted approach, which shows high and selective photocatalytic activity for the degradation of different organic dyes under UV and visible light irradiation.