A method for the determination of some pesticide residues in must and wine samples was developed using solid-phase microextraction (SPME) and gas chromatography-electron capture detection (GC/ECD). The procedure only needs dilution as sample pre-treatment and is therefore simple, fast and solvent-free. Eight fungicides (vinclozolin, procymidone, iprodione, penconazole, fenarimol, folpet, nuarim...

Regarding anti-infectious agents, no maximum residue limits are fixed for honey in the European legislation. Discussions are being conducted in order to set working limits at the European level; for example, for tetracyclines, 20 microg/kg was proposed. The Tetrasensor Honey test kit is a receptor-based assay using dipsticks for a rapid screening (30 min) of honey on the presence of tetracyclin...

We assessed ampicillin (ABPC) concentrations of kidney, muscle and intestine after a 5-day withdrawal period in 2 male and a female young Large White pigs fed the diet containing ABPC (ABPC medicated feed, 24 mg/kg/day) for a week. The ABPC residues were measured with liquid chromatography-tandem mass spectrometry, and the mean recoveries and quantitation limits ranged from 91.8 to 97.2% and fr...

A rapid method has been developed for monitoring five multiclass pesticides commonly used in citrus fruits. The determination is performed by ultra-performance liquid chromatography coupled to tandem mass spectrometry (UPLC-MS/MS), after extraction with a mixture of ethyl acetate and sodium sulfate. The method has been validated for orange matrix. Mean recoveries obtained were between 74-110% w...

A rapid, high-throughput method employing ultra-performance liquid chromatography with tandem quadrupole mass spectrometry (UPLC-MS/MS) was developed and optimized for simultaneous quantification and confirmation of 64 pesticide residues and their toxic metabolites in fruit extracts prepared by a buffered QuEChERS procedure. The total time required for UPLC-MS/MS analysis was 8 min plus 2 min f...

A simple and quick method for the determination of organophosphorus pesticides (OPs) in drinking water has been developed. After sample extraction with methylene chloride, analysis was directly carried out without further treatment using GC with a specific detector FPD on a DB-1701P column. A linear relationship between concentration and peak area was obtained within the range of 0.005 to 0.500...

the seedbed preparation and cereal residue present due to limit of maize (zea mays l.) growing period are a major challenge in double cropping after winter cereals in iran as: shahrekord. in this research, effects of various seedbed preparation methods and crop residuea managements on vegetative growth and yield of forage maize (ksc 704) were studied in a barley-maize double cropping during 200...

An analytical method for the simultaneous determination of residues of eight neonicotinoid insecticides and two metabolites in honey using LC-MS/MS was developed and validated. Two approaches of sample preparation were investigated, with the final method involving acetonitrile extraction and subsequent cleanup by dispersive solid-phase extraction (QuEChERS type). Validation was based on quintup...

local information about tillage intensity and ground residue coverage is useful for policies in agricultural extension, tillage implement design and upgrading management methods. the current methods for assessing crop residue coverage and tillage intensity such as residue weighing methods, line-transect and photo comparison methods are tedious and time-consuming. the present study was devoted t...