-Ion-exchange isotherms between hydrotalcite-like compounds (HT) of the NO3-, CI-, and SO4forms and F , 0% Br , I , OH-, SO42-, CO3 z-, and Naphthol Yellow S (NYS 2-) ions were determined, and the spacing and the width of the 003 reflection were measured as a function of HT composition. The ion-exchange equilibrium constant for HTs of monovalent anions are in the sequence OH> F > Cl > Br> NO3> ...

The influence of crystallite size on the adsorption reactivity of phosphate on 2-line to 6-line ferrihydrites was investigated by combining adsorption experiments, structure and surface analysis, and spectroscopic analysis. X-ray diffraction (XRD) and transmission electron microscopy (TEM) showed that the ferrihydrite samples possessed a similar fundamental structure with a crystallite size var...

Cellulose based polymers have shown tremendous potential as drug delivery carrier for oral drug delivery system (DDS). Hydroxyethyl cellulose (HEC) and hydroxypropyl cellulose (HPC) are widely explored as excipients to improve the solubility of poorly water soluble drugs and to improve self-life of dosage form. This work is an attempt to modulate the physicochemical properties of these cellulos...

The microstructure and mechanical properties of materials saturate to steady states after severe plastic deformation (SPD). Despite the well-known effect temperature on steady-state microstructure, there is no general agreement significance strain rate applicability Zener-Hollomon parameter in this regard. In study, several pure metals (aluminum, copper, titanium, iron) a Cu–30Zn (wt%) brass al...

This work reports on the electrochemical kinetic analysis of carbon steel powders produced during milling chips for 2, 3, and 5 h under an air atmosphere in a high-energy ball miller. aims to fill gap literature regarding transformation processes that affect powder production. information can be crucial specific metallurgy systems. The results obtained using Rietveld refinement method showed de...

ZnO nanoparticles were synthesized via novel Sol-gel route. The effects of pH variation as well as ageing were studied. The nanoparticles were synthesized with two different pH levels viz. pH 7 and pH 10. It was found that the size of the nanoparticles increased from 19 to 39.6 nm with increase in pH level from 7 to 10. Further the effect of ageing on the ZnO nanoparticles was studied. It was f...

in this research, a sol gel autocaombustion route has been proposedto synthesize alumina-zirconia composite powders, usingammonium bicarbonate as a new fuel. then the effect of calcinationtemperature on phase transformation and crystallite sizes wasinvestigated. to characterize the products xrd, tem and betanalyses were used. xrd patterns of as-synthesized powder andcalcined powders at 1100 ◦c ...

Samples with inversion parameter values (?) ranging from 0.27 to 0.14 while maintaining the crystallite size value have been successfully fabricated commercially available powders by mechanical grinding and thermal annealing treatments at temperatures between 400 600 °C. Detailed characterization studies of these samples using X-ray, neutron diffraction magnetic measurements confirmed for first...

CuO nanoparticles obtained in a low-pressure arc discharge plasma followed by annealing an oxygen atmosphere at 500°C were studied X-ray diffraction and transmission electron microscopy. The formation of irregularly shaped the size range 5–30 nm was found. Rietveld refinement confirmed monoclinic phase with average crystallite ~21 nm. temperature dependences magnetization permittivity have been...