Fine, monophasic silicon carbide powder has been synthesized by direct solid-state reaction of its constituents namely silicon and carbon in a 2.45 GHz microwave field. Optimum parameters for the silicon carbide phase formation have been determined by varying reaction time and reaction temperature. The powders have been characterized for their particle size, surface area, phase composition (X-r...

Zirconia ceramics with porous structure have been prepared by solid-state reaction using yttria-stabilized zirconia and stearic acid powders. Analysis of its microstructure and phase composition revealed that a pure zirconia phase can be obtained. Our results indicated that its porosity and pore size as well as the mechanical characteristics can be tuned by changing the content of stearic acid ...

Vanadium peroxo-citrate complex was used for the first time for synthesis of YVO4:Eu red emission phosphor material by hydrothermal method. It was found that particles size can be efficiently controlled in the range of 60–400 nm by changing concentration of the solution utilized for the hydrothermal process. The nanocrystalline powders of YVO4:Eu prepared at 200°C for 2 h with post-synthesis he...

Nanostructured Al and Al-Mg (Mg 30 wt. %) powders with the mean crystallite sizes of 42 and 11 nm were prepared through the solid state ball milling technique. The milling process was performed for various times up to 12 h in argon atmosphere and the synthesized powders were in detail characterized by different techniques. The effect of milling time and Mg addition on the size, morphology, chem...

ni6(n2h4)6(so4)4(oh)2(h2o)8](so4)(h2o)10 complex was prepared according to literature report. the reaction between aforementioned complex via sodium alkoxides as a reactants, were carried out in the solid state. the [ni6(n2h4)6(so4)4(oh)2(h2o)8](so4)(h2o)10 undergoes an intramolecular two electrons oxidation-reduction reaction at room temperature and metallic nickel nanoparticles (ni1-ni5) was ...

ni6(n2h4)6(so4)4(oh)2(h2o)8](so4)(h2o)10 complex was prepared according to literature report. the reaction between aforementioned complex via sodium alkoxides as a reactants, were carried out in the solid state. the [ni6(n2h4)6(so4)4(oh)2(h2o)8](so4)(h2o)10 undergoes an intramolecular two electrons oxidation-reduction reaction at room temperature and metallic nickel nanoparticles (ni1-ni5) was ...

Preparation and properties of La(Cr0.2Mn0.2Fe0.2Co0.2Ni0.2)O3 high-entropy ceramics are investigated. prepared by a traditional two-step solid-state reaction method in air. single-phase powders synthesized calcining the mixed oxides at 1000 °C for 20 h. The sintered 1350–1650 muffle furnace 4 h using above powders. phase compositions different temperatures characterized X-ray diffraction (XRD) ...

Mechanical alloying (MA) is a solid-state powder processing technique involving repeated cold welding and fracturing of powder particles in a high-energy ball mill. It has been used to obtain nanocrystalline binary system FeNi. Fe and Ni elemental powders have been ball milled in a planetary mill (Pulverisette5, Fritsch) for various times up to several hours. The morphology of the powders was e...