2-(pyridine-2-yl)-N-p-chlorohydrazinecarbothioamide (HCPTS) was synthesized, characterized and successfully applied for the preconcentration of Cu(II), Ni(II), Zn(II), Cd(II), Co(II), Pb(II), Fe(II), and Hg(II) in water, blood, and urine samples prior to graphite furnace atomic absorption determination (GFAAS); Hg was determined by cold vapor technique. Under the optimum experimental conditions...

a simple, highly sensitive, accurate and selective method for determination of trace amounts of cu2+ in water samples .in this paper, chitosan was used to encapsulate nano-fe3o4 and produce a nano-fe3o4-chitosan sorbent based new sorbent was prepared. this was treated with ethylenediamine (ed) in another solvent-free procedure for the formation of a novel nano-fe3o4-chitosan-ed.flame atomic abs...

A simple and reproducible method for the rapid extraction and determination of trace amounts of copper (II) ions using octadecyl-bonded silica membrane disks modified by Functionalized Graphene with octadecylamine (ODA–GO) and Atomic Absorption Spectrometry is presented. The method is based on complex formation on the surface of the ENVI-18 DISK TM disks followed by stripping of the retained sp...

Membrane separation is a very well known technology having a large number of applications. Separation of metal ions by selective membrane transport is of great importance from both fundamental and practical viewpoints. According to IUPAC, a membrane is defined as a heterogeneous phase which acts as a barrier to the flow of molecules and ionic species in liquid or vapour phase. Membranes can be ...

A preconcentration system for multi-element electrothermal atomic absorption spectrometry was developed with a microcolumn packed with a chelating resin. The proposed method was applied successfully to the simultaneous determination of Co, Ni and Cu in seawater. A sample volume of 2 ml was required for the analysis. Retention of metal ions as a complex on the microcolumn was achieved by using M...

This article reports on an investigation into the ability of minced banana peel to extract lead and copper ions from water and the parameters involved in this process. The kinetics of copper and lead uptake reached equilibrium in 10 min and the extraction of metals ions was favorable above pH 3. The medium was characterized by FTIR, which showed absorption bands of carboxylic and amine groups a...

A method for the preconcentration and determination of cobalt in human urine samples was developed. The online preconcentration and determination were attained using inductively coupled plasma atomic emission spectromety (ICP-AES) coupled to a flow injection (FI) method. Cobalt was retained on an Amberlite XAD-7 resin as cobalt-2-(5-bromo-2-pyridylazo)-5-diethylaminophenol complex at pH 9.5. Co...

A novel and selective method for the fast determination of trace amounts of Cu(II) ions in water samples has been developed. The procedure is based on the selective formation of Cu(II) at optimum pH by elution with organic eluents and determination by flame atomic absorption spectrometry. The method is based on complex formation on the surface of the ENVI-18 DISKTM disks modified Schiff base-ch...