in this paper cufe2o4, nanocrystalline powders were prepared. also, the supported cu ferrite was obtained by impregnation of the supports with cu and fe nitrates solutions, for calcination temperature 450 ºc. the samples were characterized by x-ray powder diffraction (xrd) and fourier transform-infrared spectroscopy (ft-ir). photocatalytic degradation of acid red 206 in water was studied. cufe2...

Y2O3:Eu were prepared through precursors synthesized by leaching tests, removing impurities, enrichment of Y and Eu from residual purified liquors, annealing treatment, and high temperature solid-state reaction method, which is the most suitable for large-scale production. The analysis of product shows that the purity is 99.42%. The resultant powders were characterized by X-ray diffraction (XRD...

Improved powders for capturing CO2 at high temperatures are required for H2 production using sorption-enhanced steam reforming. Here, we examine the relationship between particle structure and carbonation rate for two types of Na2 ZrO3 powders. Hollow spray-dried microgranules with a wall thickness of 100-300 nm corresponding to the dimensions of the primary acetate-derived particles gave about...

Lithium nickel oxide (LiNiO2) powders with an R3 m structure are successfully synthesized via a developed reverse microemulsion process. This method can effectively reduce the calcination temperature for synthesizing monophasic LiNiO2 powders to 700 C, which is much lower than that in the solid-state process. Nanosized LiNiO2 powders with narrow particle size distribution are obtained via the m...

In this study, BaZrO3:Eu0.025 powder was synthesized through the solid-state reaction method with two different heating processes. For the one-step process, the BaZrO3:Eu0.025 powder was heated to 1000 ̋C–1400 ̋C for 2 h. For the two-step heating process, the BaZrO3:Eu0.025 powder was pre-heated at 800 ̋C for 2 h, after being cooled to room temperature and ground, then the powder was heated to ...

In situ x-ray diffraction was used to optimize the synthesis of Aurivillius structure ceramic powders. Powders were prepared via conventional solid-state synthesis and the Pechini polymer precursor method. The phases Bi4Ti3O12, and Bi2Sr2Nb2TiO12 were studied. The Bi4Ti3O12 phase formed easily, regardless of processing route, between 400-500C and phase purity was achieved by 700C when using the...