نتایج جستجو برای: determination of cu preconcentration
تعداد نتایج: 21179627 فیلتر نتایج به سال:
On-line system incorporating a microcolumn of Muromac A-1 resin was used for the developing of method for preconcentration of trace elements followed by inductively coupled plasma (ICP) atomic emission spectrometry determination. A chelating type ion exchange resin has been characterized regarding the sorption and subsequent elution of 24 elements, aiming to their preconcentration from water sa...
Polychlorotrifluoroethylene (PCTFE) in the form of beads was applied, as packing material for flow injection on-line column preconcentration and separation systems coupled with flame atomic absorption spectrometry (FAAS). Its performance characteristics were evaluated for trace copper determination in environmental samples. The on-line formed complex of metal with diethyldithiophosphate (DDPA) ...
a simple and reproducible method for the rapid extraction and determination of trace amounts of copper(ii) ions using octadecyl-bonded silica membrane disks modified by 1-(2-pyridyl azo)2-naphtol(pan) and atomic absorption spectrometry was presented. the method was based on complex formation on the surface of the envi-18 disk tm disks followed by stripping of the retained species by minimum amo...
In the present study, a simple and efficient extraction method based on dispersive liquid-liquid microextraction prior to UV-Vis spectrophotometry was developed for the preconcentration and determination of copper ions in environmental samples. Briefly, cupric ions (Cu II) were reduced to cuprous (Cu I) with addition of hydroxyl amine hydrochloride and formed hydrophobic chelates with neocuproi...
A method for the preconcentration and determination of Cr(III), Co(II), Cu(II), Fe(III) and Pb(II) ions by atomic absorption spectrometry has been described. The method was based the collection of metal-calmagite complexes on a soluble cellulose nitrate membrane filter. The detection of the solution was obtained by flame atomic absorption spectrometry (FAAS) after completely dissolving the memb...
The aim of this work was to develop a new and simple coacervative extraction method for the preconcentration and spectrophotometric determination of Cu(II) in water samples. Dithizone was used as the chelating agent while an anionic surfactant, namely sodium dodecyl sulfate (SDS), was used as extracting agent at room temperature. Central composite design (CCD) based on response surface methodol...
Numerous instrumental methods are used to determine heavy metals in natural water, mainly with preconcentration, since the sensitivity of direct analysis is often insufficient. A number of such methods have been developed in the authors' laboratory. Highly selective solvent extraction separation of heavy metals (Ag, Cu, Hg) has been achieved by using macrocyclic extractants. The separated eleme...
The widespread use of silver compounds and silvercontaining procedures in industry, medicine, jewellery, cloud seeding and in disinfection of drinking water has resulted in an increasing silver content in environmental samples. Silver impregnated filters are used in water disinfection, while silver concentrations up to 200 μg L are permitted for antimicrobial activities for human health. Silver...
The anodic stripping voltammetric determination of gold was accomplished on a chemically modified glassy carbon electrode in a solution containing chloride ions. A modifying polymer, polyvinylferrocene, was coated by immersing the glassy carbon surface in its solution in methylene chloride followed by solvent evaporation. Tetrahalo complexes of gold, tetrachloroaurate(III) and tetrabromoaurate(...
Synthetic resin, Amberlite XAD-4 was linked covalently with the third generation supramolecule, octa-O-methoxy resorcin [4] arene through -N=Ngroup to form chelating resin, which has been characterized and effectively used for the separation and preconcentration of metal ions such as Ni(II), Cu(II), Zn(II) and Cd(II). Critical parameters such as pH, flow rate, sorption capacity, breakthrough st...
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