نتایج جستجو برای: headspace solid phase microextraction

تعداد نتایج: 755834  

Journal: :Journal of chromatography. A 2003
Brett J Savary Alberto Nuñez

A simple, fast, and direct procedure was developed for the simultaneous determination of the methanol and acetic acid present as esters in the plant cell wall polysaccharide pectin. After base-hydrolysis of esters and acidification of pectin samples, headspace solid-phase microextraction (SPME) was performed using a Carboxen-PDMS fiber assembly. Methanol and acetic acid were separated by gas ch...

Since solid-phase and liquid-phase microextraction (SPME and LPME) were introduced, as effective solvent-free methods, many efforts have been made to improve their modes and applications. However, due to limitations with sensitivity and efficiency, researchers have focused on improving the performance of their basic primary modes. In this way, in recent years, different methods such as ultrason...

2006
Yan Wang

The use of laser desorption as a sample introduction method for solid-phase microextraction (SPME) has been investigated in this research project. Three different types of analytical instruments, mass spectrometry (MS), ion mobility spectrometry (IMS) and gas chromatography (GC) were employed as detectors. The coupling of laser desorption SPME to these three instruments was constructed and desc...

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