نتایج جستجو برای: xrd sem
تعداد نتایج: 77043 فیلتر نتایج به سال:
در این تحقیق نانو ذرات ابررسانای ybco با استفاده از روش ترکیبی سل-ژل، احتراقی با اندازه متوسط 100 نانو مترساخته شدند و اثر تغییرph سل و تغییر دمای پخت بر تشکیل فاز ابررسانایybco و بر اندازه ذرات این ابررسانا مورد بررسی قرار گرفت. دو دسته نمونه از سل های با ph، 7 و 5 تهیه شد. دمای پخت 880 درجه سانتیگراد انتخاب و به مدت 5 ساعت در دمای مذکور حرارت دهی شدند. با استفاده از پراش اشعه x (xrd) و میکروس...
in this paper, plate-like nio nanoparticles were prepared by one-pot solid-state thermal decomposition of nickel (ii) schiff base complex as new precursor. first, the nickel (ii) schiff base precursor was prepared by solid-state grinding using nickel (ii) nitrate hexahydrate, ni(no3)2∙6h2o, and the schiff base ligand n,n′-bis-(salicylidene) benzene-1,4-diamine) for 30 min without using any solv...
the austenitic stainless steel (ss) has been used as a material for building ultra high vacuum (uhv) chamber. recently significant efforts have been concerned a comparing the standard cleaned for ultra high vacuum, passivity stainless. in this work austenitic nanocomposites were synthesize by sol- gel method. the morphologies and topographies of the samples have b...
the dried nitrate-urea gels exhibit the combination of autoicatatric combustion behavior and ultrasonic, whichcan be used to synthesize the nanocatalyst ferrite powders. cu and ni unites nanocatalyst powders sithcomposition of caned], and nife204 were synthesized by a sol-gel auto catalnic combustion process. themolar ratio between metal ions and urea was 11.2. the sob gel process was done at 8...
In this paper, we have reported convenient way to access CdTe nanorods by solvothermal decomposition using single source molecular precursor cadmium (II) bis-(isopropyl telluro) propane (SSMP) and quinoline as solvent at relatively low temperature (200oC).As synthesized nanomaterials are structurally characterized by XRD, SEM and UVVisible spectroscopy. SEM micrographs revealed formation of rod...
silver nanoparticles with size of 6- 57nm were synthesized by bioreduction method from anisochilus carnosus aqueous and ethanolic extract. biosynthesized nanoparticles showed maximum antimicrobial activity against k. pneumonia (13±1.67mm), e.coli (13±1.97mm) and b. subtilis (13±1.07mm) followed by p. aeruginosa and minimum against s. aureus. the quantitative formation, characteristics and impur...
the combustion process of tio2- 2mg- c and 3tio2-4al-3c systems in a tubular furnace was investigated. tic has been synthesized by the magnesiothermic reaction from a mixture of compacted powders of tio2, mg and charcoal as starting materials in the presence and absence of nacl. the effects of temperature, pressure, and the stoichiometry ratio in the reaction yield have been studied. the result...
امروزه علاوه بر تعیین شاخص های شیمیایی ذرات گردو غبار، بررسی ویژگیهای فیزیکی و نقش آنها در آلودگی محیط زیست نیز حائز اهمیت است. در این راستا تعداد 10 نمونه برداشته شده در سالهای 1387 و 1388در روزهای گرد و غباری با خاستگاه فرا محلی در استان خوزستان برای بررسیهای کانیشناسی و ریختشناسی مورد بررسی xrd و sem قرار گرفتند. نتایج حاصل از بررسیهای xrd نشان داد که ترکیب کانی شناسی ذرات گرد و غبا...
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