nano-sized batio3 powders with particular nb concentrations were prepared by rotary- hydrothermal (rh) method. hydrothermal method was used at 180 °c for 5 hours with new ti pressure and the teflon vessel was rotated at a speed of 160 rpm during the hydrothermal reaction. new hydrothermal method was used instead of previous solid state reaction for the system batio3±nb2o3 in high temperature to...

The SrAl2O4: Eu 2þ, Dy3þ phosphor powders were prepared by a new sol–gel method using aluminum isopropoxide and strontium acetate as precursors. The sol–gel process and the structure of the phosphor powders were investigated by means of DSC-TG and XRD. It was found that the single-phase SrAl2O4 was formed at 900 8C, which is 300 8C lower than that required for the conventional solid-state react...

the nanopowders of sno2, casno3 and ca2sno4 in the size rang of 5-70 nm have been prepared using solid-state reaction technique. the technique is convenient and inexpensive in comparison to the conventional routes of compound prepared and processing where, many steps of mixing and annealing are involved. formation of resultant compounds was explained on the basis of reaction taken place between...

Nanostructured Mn2Sb2O7 powders were synthesized via stoichiometric1:1 Mn:Sb molar ratio solid state reaction at different reactions temperatures for 8 h using MnSO4.H2O and Sb2O3 as raw materials. The synthesized materials were characterized by powder X-ray diffraction (PXRD) technique. Structural analyses were performed by the FullProf program employing profile matching with constant scale fa...

A basic alumina-spinel low cement castable (LCC) composed of sintered bauxite, reactive alumina, calcined alumina, calcined magnesia, microsilica, and high alumina refractory cement was prepared (castable A) to which 5% sodium hexa-meta phosphate was later added (castable B) to prepare samples for heat treatment at 110ºC, 900ºC, and 1400ºC. Bulk Density (BD), Apparent Porosity (AP), and Cold Cr...

Nano-sized BaTiO3 powders with particular Nb concentrations were prepared by Rotary- Hydrothermal (RH) method. Hydrothermal method was used at 180 °C for 5 hours with new Ti pressure and the teflon vessel was rotated at a speed of 160 rpm during the hydrothermal reaction. New hydrothermal method was used instead of previous solid state reaction for the system BaTiO3±Nb<sub...

Nano-sized BaTiO3 powders with particular Nb concentrations were prepared by Rotary- Hydrothermal (RH) method. Hydrothermal method was used at 180 °C for 5 hours with new Ti pressure and the teflon vessel was rotated at a speed of 160 rpm during the hydrothermal reaction. New hydrothermal method was used instead of previous solid state reaction for the system BaTiO3±Nb<sub...

The NbSe2 nanoplates with novel hexagonal morphology have been obtained via solid-state assembly of NbSe2 ultrathin nanosheets, which were prepared by a simple calcination process using micro-sized Nb and Se powders as the precursors. The influence of high-temperature annealing upon morphology of single-crystal NbSe2 was investigated. On the basis of experimental results of different temperatur...