The structure of nano-crystalline Fe2O3 particles, synthesized using the microwave plasma technique, has been analysed using synchrotron based X-ray absorption spectroscopy and X-ray powder diffraction, as well as transmission electron microscopy. Furthermore, magnetic properties, the crystal structure, and the microstructures are compared and the potential model character of the samples for st...

We have investigated spin-wave excitations in rolled-up Permalloy microtubes using microwave absorption spectroscopy. We find a series of quantized azimuthal modes which arise from the constructive interference of Damon-Eshbach-type spin waves propagating around the circumference of the microtubes, forming a spin-wave resonator. The mode spectrum can be tailored by the tube's radius and number ...

This compilation of work includes four aspects: (1) an academic review on the significance and implementation of Quality by Design (QbD), (2) mechanistic studies on the palladium-catalyzed synthesis of diarylmethanes, (3) the optimization of microwave-assisted click reactions and Suzuki couplings for use in an undergraduate organic chemistry laboratory manual, and (4) monitoring the progress of...

Dialkyl 1,4-dihydro-2,6-dimethylpyridine-3,5-dicarboxylates have been prepared in a batch mode under conventional heating as well as under continuous flow conditions in the Miniflow 200SS, Sairem's microwave-assisted batch and continuous flow equipment. Real-time monitoring of the reactions by Raman spectroscopy enabled to compare both heating modes and to determine (optimized) reaction times.

The Bi2O2CO3 (BOC) samples were successfully synthesized by a microwave-assisted method at different microwave powers and lengths of irradiation time. as-synthesized characterized X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), transmission (TEM), photoluminescence (PL) UV–visible spectroscopy. analytical results demonstrated that the...

Mobilities and lifetimes of photogenerated charge carriers are core properties photovoltaic materials can both be characterized by contactless terahertz or microwave measurements. Here, the expertise from fifteen laboratories is combined to quantitatively model current-voltage characteristics a solar cell such To this end, impact measurement conditions, alternate interpretations, experimental i...

using C02 laser difference generation in metal-insulator-metal diodes either from the difference between a fixed frequency C02 laser and a tunable waveguide laser, or from the difference between two fixed frequency C02 lasers plus microwave sidebands. is being used to make highly accurate FIR frequency measurements of stable species to serve as frequency and wavelength calibration standards; to...