نتایج جستجو برای: in situ forming sol gel
تعداد نتایج: 17010565 فیلتر نتایج به سال:
nanocrystalline complex oxides have been synthesized by combination of sol–gel auto combustion and ultrasonic irradiation techniques using copper nitrate, zinc nitrate as metallic nitrates and glycine, urea and thiourea as fuels. sol-gel combustion (combination of the chemical sol–gel process and the combustion process) as a proper synthesized technique is used to synthesize zno/cuo nanocomposi...
هدف از انجام این پروژه سنتز نانوکریستال زیرکونیا با روش سل-ژل اصلاح شده و سنتز نانوکریستال زیرکونیای سولفاته با استفاده از یک روش سنتز و یک نمک زیرکونیوم جدید بود. برای سنتز نانوکریستال زیرکونیا، در مرحله اول یک سل با استفاده از پیش ماد? زیرکونیوم -nپروپوکساید در مجاورت آب و آمونیاک ساخته شد و گلوکز و فروکتوز به عنوان دو افزایند? آلی با نسبت یک به یک به محلول اضافه شدند. ژل ایجاد شده به مدت 12 ...
incorporation of copper species into silica matrix was performed by the sol-gel method. copper ions and copper particles were doped using two different copper sources; cu(no3)2.3h2o and copper particles chemically synthesized.the particles of copper metallic, cuprous and cupric oxide were prepared and the synthesis and characterizations of copper species were compared together. on the other han...
This paper describes the synthesis of Pb(Zr0.95Ti0.05)O3 powder by sol gel and solid state methods. PZT powders were fabricated by solid-state reaction process using metal oxides and in sol gel method salts and organic compounds were employed. The powders were calcined at 700 and 950 oC in sol gel and solid state methods, respectively. The synthesized powders were analyzed by FTIR and XRD. Th...
Sol–gel chemistry is an efficient tool to control the morphology and reactivity of solids. Drying is the crucial step due to the capillary forces exerted during the classic ambient drying process, which induces the collapse of the wet gel porosity. The use of N, N-dimethylformamide (DMF), a newly found DCCA were found to be effective in the sol–gel synthesis of crack-free silica gel monolith fr...
This paper presents experimental analysis and results of GaN (being a III-V semiconductor) doped with Ferrite elements synthesized using Sol-Gel technique which are carried out at National Chemical Laboratory, Pune Maharashtra. The GaN is employed as dopant for x=1 and x=5, in the formula Ga(2x) N Fe2(49-x) O3 . A non-spinel ferrite system ( Fe2 O3) is chosen for our study. The XRD (Structural)...
CoTiO3-clay nano-composites were synthesized via a conventional sol-gel method; the gel was calcinated at 500 - 800°C for 2 hours. The presence of rhombohedra phase of CoTiO3 in clay matrix was confirmed by XRD, FTIR, SEM. Cobalt titanate-clay nano-composites were prepared with 5-20%(w/w) by sol-gel method. The spectra results were investigated at 20% (w/w) concentration .The optimum condition ...
Microencapsulation has become a hot topic in chemical research. Technology mainly used for control release and protection purposes. The sol-gel micro encapsulation approach for fragrance and aroma in porous silica-based materials leads to sustainable odorant and flavored materials with novel and unique beneficial properties. Sol-gel encapsulation of silica based micro particles considered econo...
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