A novel ICP-OES method has been developed for the determination of Si concentration, originating from polyorganophosphosilanes, in biological specimens that also contain metal ions. The is free hazardous hydrofluoric acid (HF) and involves digestion with HNO3/H2O2 prior to analysis by ICP-OES. High reproducible spike recovery was obtained controls.

We developed a rapid acid-digestion method for preparing tissue samples for iron determination. Specimens were digested in nitric acid and hydrogen peroxide under high temperature and pressure in closed Teflon vessels, with microwave energy. Analysis for iron in 25- to 250-mg portions of digested bovine liver powder (National Bureau of Standards Certified Reference Material no. 1577a) showed ex...

The complete amino acid sequence of hen ovalbumin, comprising 385 residues, has been determined. The sequence was deduced from the 17 cyanogen bromide fragments and from peptides derived by digestion with a number of proteolytic enzymes. The molecular weight of the polypeptide chain of ovalbumin is 42699. Ovalbumin has four sites of postsynthetic modification; in addition to the acetylated N te...

Human neuropeptide Y was isolated from acid extracts of adrenal-medullary phaeochromocytoma tissue. After (NH4)2SO4 fractionation, the neuropeptide Y-like immunoreactivity was purified from the resolubilized 80%-saturation-(NH4)2SO4 peptide-rich precipitate, by gel filtration, cation-exchange chromatography and reverse-phase high-pressure liquid chromatography. Amino acid analysis of the peptid...

Anaerobic digestion is an engineered methanogenic decomposition of organic matter under oxygen-free conditions and involves a mixed consortium of different species of anaerobic microoganisms that transform organic matter into biogas. The process is successfully used for the treatment of municipal sludge, animal manure, industrial sludge, and industrial and municipal wastewaters. Applications of...

Acid hydrolysis is a key process for the production of platform chemicals from biomass, however solid residues by-products can amount to 50 wt% starting biomass material. In this study, biofuel precursor levulinic acid were generated via microwave-assisted Miscanthus x Giganteus and investigated supplementation anaerobic reactors digesting Chicken Manure. The addition increased methane yields b...

A rapid sample-digestion method for the determination of toxic metals, cadmium, chromium, and lead, in polyethylene and polyvinyl chloride has been developed by using a microwave oven for household use. An appropriate amount of the sample taken in a PTFE decomposition vessel was mixed with nitric acid or nitric and sulfuric acids. The vessel was heated in a microwave oven by a predetermined ope...