A method for measurement of dimensions of platy particles of exfoliating, or delaminating, materials, such as clays, in aqueous suspensions in situ is proposed. Equivalent spherical diameter (esd), measured by many common methods, depends more on the major (lateral) dimension of a particle, while it is less sensitive to changes of the particle thickness. Addition of the second method, results o...

A Cu−carborane-based metal−organic framework (MOF), NU-135, which contains a quasi-spherical para-carborane moiety, has been synthesized and characterized. NU-135 exhibits a pore volume of 1.02 cm/g and a gravimetric BET surface area of ca. 2600 m/g, and thus represents the first highly porous carborane-based MOF. As a consequence of the unique geometry of the carborane unit, NU-135 has a very ...

A review of production of activated carbon from waste tire char is presented. This review compiles the work done by various researchers on the characterisation of activated carbon from tire char and its applications in liquid-phase adsorption. Effect of various process parameters particularly activation temperature, burn-off, surface area on the activation stage are reviewed. Influence of activ...

In this study, the synthesis and structural properties of a Molecularly Imprinted Polymer (MIP) and a Nonimprinted Polymer (NIP) bearing Fe-porphyrin moiety and amino acid moieties including Histidine (His), Tryptophan (Trp) and Arginine (Arg) are presented. The imprinted and nonimprinted polymeric beads were synthesized by suspension polymerization technique and characterized by using FT-IR sp...

A highly porous porphyrin-based organic polymer, PCPF-1, was constructed via homo-coupling reaction of the custom-designed porphyrin ligand, 5,10,15,20-tetrakis(4-bromophenyl)porphyrin. PCPF-1 possesses a large BET surface area of over 1300 m(2) g(-1) (Langmuir surface area of over 2400 m(2) g(-1)) and exhibits strong hydrophobicity with a water contact angle of 135°, and these features afford ...

The research objective was to produce activated carbon from palm-oil shells by one step pyrolysis and steam activation in a fixed bed reactor with the diameter of 100 mm. The studied variables were activation temperature, activation time, palm-oil shell sizes and flow rate of air. The results showed that the optimum condition was 1.18-2.36 mm of palm-oil shells at 750C for 2 hr with air flow ra...

Easily prepared nanoZnO was found to be as an efficient catalyst in the synthesis of 1,4-DHPs via four-component reaction of 1,3-dicarbonyls, aldehydes and ammonium carbonate in water at 60 °C. The prepared nanoZnO was characterized by XRD and FT-IR analysis, while the determined specific surface area of nano catalyst by BET method was 33 m2/g.

Easily prepared nanoZnO was found to be as an efficient catalyst in the synthesis of 1,4-DHPs via four-component reaction of 1,3-dicarbonyls, aldehydes and ammonium carbonate in water at 60 °C. The prepared nanoZnO was characterized by XRD and FT-IR analysis, while the determined specific surface area of nano catalyst by BET method was 33 m2/g.

using fe(no3)3.9h2o, co(no3)2.6h2o and mn(no3)2.4h2o the magnetic properties of nanoparticles trimetalic iron - cobalt - manganese, with supported magnesium oxide have been prepared by co-precipitation and solvothermal methods. the prepared samples are characterized by scanning electron microscope (sem), x-ray diffraction (xrd), vibrating sample magnetometer (vsm) and brunaer-emmett-teller (bet...