*Correspondence: P. Chen, Department of Chemical Engineering and Waterloo Institute for Nanotechnology, University of Waterloo, 200 University Avenue West, Waterloo, ON N2L3G1, Canada e-mail: [email protected] Lithium-rich layered powders, Li2MnO3-stabilized LiMO2 (M=Ni, Co, Mn), are attractive cathode candidates for the next generations of high-energy lithium-ion batteries. However, most of ...

Based on precursor powders with a size of 200-300 nm prepared by the low-temperature solid-state reaction method, phase-pure YMnO₃ ceramics are fabricated using spark plasma sintering (SPS). X-ray diffraction (XRD) and scanning electron microscopy (SEM) reveal that the high-purity YMnO₃ ceramics can be prepared by SPS at 1000 °C for 5 minutes with annealing at 800 °C for 2 h. The relative densi...

Abstract The possibilities of improving the crystallization and optical properties strontium europium oxonitridosilicate phosphor powders were discussed. Two different routes synthesis presented: traditional solid-state reaction method gas pressure synthesis. It was proven that altering partial during process enhances a desired single, triclinic SrSi 2 O N phase. XANES measurements confirmed co...

The Fe-Ni-Sb-B amorphous alloy has been prepared by a solid-solid chemical reaction of ferric trichloride, nickel chloride, antimony chloride and potassium borohydride powders at room temperature. The inductive couple plasma study indicates that the resultant is composed of Fe 5.38 %, Ni 56.19 %, Sb 29.02 % and B 0.44 %. The XRD and thermal analysis show that the alloy is a non-strict sense amo...

The aim of this study is to investigate the effect of the sintering schedule on microstructure and properties of hydroxyapatite which is produced by different synthesizing methods. Hence, wet-chemical precipitation and solid-state reaction were performed to prepare nano-sized hydroxyapatite (HA) powders. Powders were then uniaxially pressed and sintered by varying temperatures and times. XRD an...

Synthesis The compounds were prepared by the solid state reaction of Cu, Zn, Sn, and S powders in the appropriate ratios in evacuated, sealed, fused silica tubes. They were heated at 750 °C (ramp 300 °C/h) for 170 h and then cooled down at 20 °C/h. The obtained powders were then ground and pressed into pellets which were again put into a sealed tube. The second heating sequence was: ramp 300 °C...

The solid state reactions and structural evolution in nanocrystalline FePt powders during mechanical ball milling at 77 K and subsequent annealing have been investigated. Above 310 °C the formation of L10 FePt is observed. As the milling time increases, the enthalpy evolved during the transformations is reduced, whereas the corresponding activation energy increases. For accelerating the orderin...