One-step facile synthesis of monoporous polymer microspheres via microwave-controlled dispersion polymerization is introduced. This template-free method employing the dispersion polymerization of styrene under microwave irradiation induces directly the formation of uniform monoporous polymer microspheres, with controllable morphologies and sizes, which can be tuned by simply adjusting parameter...

Mechanically Activated Self-propagating High temperature Synthesis (MASHS) is the method which is used to promote self-propagating synthesis by increasing activity of reactants and increase the purity of products. In this study Ti 2 AlC and Ti3AlC2 max phases were synthesized by using mechanically activated self-propagating high temperature synthesis (MASHS) and samples reactivity and phase str...

A rapid and efficient method for the synthesis of bis-thiazolidinones has been achieved by pseudo five-component reaction of aldehydes, ethylenediamine and thioglycolic acid in the presence of nano-NiZr4(PO4)6 as catalyst under microwave irradiation. Nano-NiZr4(PO4)6 has been characterized by powder X-ray diffraction, scanning electronic microscopy (SEM), energy dispersive spectroscopy (EDS), v...

Present work describes the synthesis of coumarin Mannich bases 4-7 by the application of Mannich reaction on 7-hydroxy-4-methyl coumarin 3 using conventional as well as microwave technology to compare the feasibility, reaction time and yield of the product. For this, 7-hydroxy-4-methyl coumarin 3 was prepared using Pechmann condensation reaction and Mannich bases (4-7) were synthesized by the r...