نتایج جستجو برای: powders solid state reaction
تعداد نتایج: 1387945 فیلتر نتایج به سال:
— α-Ba2ZrF8 is prepared as systematically twinned crystals by hydrothermal synthesis (200°C) or as fine powders either on a sand bath (60°C) (aqueous HF medium) or by solid state reaction at 450°C. Synchrotron radiation was used because of ambiguities in indexations from conventional X-ray (pseudo-hexagonal symmetry). The structure was determined ab initio from synchrotron powder data. Neutron ...
Unprecedented rhodium-catalyzed stereoselective polymerization of "carbenes" from ethyl diazoacetate (EDA) to give high molecular mass poly(ethyl 2-ylidene-acetate) is described. The mononuclear, neutral [(N,O-ligand)M(I)(cod)] (M = Rh, Ir) catalytic precursors for this reaction are characterized by (among others) single-crystal X-ray diffraction. These species mediate formation of a new type o...
Based on precursor powders with a size of 200-300 nm prepared by the low-temperature solid reaction method, phase-pure YFeO₃ ceramics are fabricated using spark plasma sintering (SPS) at different temperatures. X-ray diffraction (XRD) and scanning electron microscopy (SEM) reveal that the high-purity YFeO₃ ceramics can be prepared using SPS, while the results from X-ray photoelectron spectrosco...
Preparation of Soft Magnetic Fe-Ni-Pb-B Alloy Nanoparticles by Room Temperature Solid-Solid Reaction
The Fe-Ni-Pb-B alloy nanoparticles was prepared by a solid-solid chemical reaction of ferric trichloride, nickel chloride, lead acetate, and potassium borohydride powders at room temperature. The research results of the ICP and thermal analysis indicate that the resultants are composed of iron, nickel, lead, boron, and PVP, and the component of the alloy is connected with the mole ratio of pota...
In this research fly ash (FA) from Iran Ferrosilice Company was converted to zeolite A by hydrothermal procedure. The type and quality of produced zeolite depends on the composition of used FA, concentration of sodium hydroxide solution, and parameters such as temperature, reaction time and liquid/solid ratio. The fly ash was fused with sodium hydroxide at 550°C for 1 hour followed by dissoluti...
in order to gain a better understanding of the chemistry of methanl-to-hydro-carbon conversion, it is necessary to determine the nature of the primary reaction products. experiments carried out in this work on h-zsm-11, using a continuous flow reactor linked to an on-line gas chromatograph demonstrated that ethylene and methane are the primary reaction products. the results obtained using solid...
The effect of sintering condition on structure, microstructure, and ferroelectric properties ([Formula: see text][Formula: text] text]- O 3 (KNL–NTS) has been investigated. Ceramic powders have synthesized by the solid-state reaction method sintered at different temperatures (1115[Formula: text]C, 1125[Formula: 1140[Formula: text]C). Then, samples were characterized thermogravimetric analysis, ...
One of the characteristics of solid organic compounds and especially organic explosives is thermal behavior and kinetic of thermal decomposition. The activation energy, Arrhenius constant and model of solid state reaction as kinetic triplet can be obtained by study thermal decomposition kinetic in a solid state reaction. In the present work, the non-isothermal differential thermal analysis (DTA...
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