Microwave-assisted extraction (MAE) and microwave-assisted hydrolysis (MAAH) were developed for the sample preparation of guava leaves prior to GC determination of quercetin and its glycosides. Ethanol was selected as the solvent. The optimum MAE temperature, particle size, solvent volume and MAE time are 120 degrees C, 40 - 60 mesh, 20 mL and 5 min, respectively; the optimum MAAH temperature a...

─ Upgrading successful processes of microwave-assisted organic synthesis to the level of industrial technology is currently slowed by difficulties in experimental development of largescale and highly-productive reactors. This paper proposes to address this issue by developing microwave chemistry reactors as microwave systems, rather than as black-box-type units for chemical reactions. We sugges...

Microwave-assisted double decarboxylative Claisen rearrangement of bis(allyl) 2-tosylmalonates provides substituted 1,6-heptadienes, which may be alkylated, and then converted into pyridines by ozonolysis followed by reaction with ammonia generated in situ under microwave conditions.

Tungsten oxide (WO3) and tungsten oxide hydrate (WO3.H2O) nanoparticles were synthesized via microwave-assisted solution combustion in comparison with the acidic precipitation method. Oxalic acid was used as a surfactant and forming agent in the acidic precipitation method. In addition to oxalic acid, glycine and citric acid were also used as fuels in the microw...

< p>In this communication, we have reported that the Pd(OAc)2–Et3SiH-DMF system promotes the microwave-assisted chemoselective reduction of aryl α,β-unsaturated esters in good yields. The protocol affords a convenient reduction of aryl-conjugated double bonds even in presence of other functional groups like esters, phenols, and ethers.

this paper focused on a simple approach for synthesis of molybdenum oxide (moo3) nanoparticles and reports a facile route for synthesis of such nanoparticles, using microwave irradiation as a homogenous and powerful source of heating, using ethylene glycol as the solvent and heating medium. for more investigations, besides microwave heating, the obtained solutions were also treated by conventio...

the effect of pre-treatments in combination with hot air, vacuum and hot-a microwave drying methods the progress of the drying process, and textural, and colour and rehydration rate on button mushroom (agaricus bisporus) slices were investigated. in this work, one of the following methods: hot air, vacuum drying or microwave-assisted convective drying and also different pre-drying treatments, v...

Present study was based upon the phytochemical screening, antimicrobial and antithrombotic potential of a traditional herb Spharenthus indicus (commonly called East Indian globe thistle). A range of solvents from non-polar to polar (n-hexane, ethyl acetate, methanol) were used to attained the extract by employing conventional and modern methods of extraction like orbital shaker assisted extract...

Microwave assisted combustion synthesis is used for fast and controlled processing of advanced ceramics. Single phase and sinter active nano crystalline alpha alumina powders were successfully synthesized by different fuel-to-oxidant molar ratios using aluminium nitrate as an oxidiser, glycine as a reducing agents and millipore water as a solvent by microwave assisted combustion synthesis. Ther...