Stress Corrosion Cracking Detection of Sensitized Stainless Steel 304 in Chloride Media by Using Electrochemical Impedance Spectroscopy (EIS)
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Abstract:
Electrochemical impedance spectroscopy (EIS) was used to detect stress corrosion cracking (SCC) in stainless steel 304 alloy exposed to an aqueous environment at 120 °C. Stainless steel 304 alloy as u-bend was tested in the solution that contains 40 weight percent of magnesium chloride. U-bended samples were prepared according to ASTM G30. EIS measurements were always performed simultaneously on u-bend samples under stress and non-stress conditions. The results indicate that changes in phase shift versus time could be related to the stress corrosion cracking process. Stress corrosion cracking is detectable at a frequency of 23.95 Hz. EIS measurement can be used for SCC monitoring in u-bend samples. Finally, analysis of the fracture surface by using metallographic and SEM techniques confirmed the EIS results.
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Journal title
volume 2 issue 1
pages 55- 60
publication date 2012-01-11
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