Effect of Morphology on the Photocatalytic Behavior of ZnO Nanostructures: Low Temperature Sonochemical Synthesis of Ni Doped ZnO Nanoparticles
Authors
Abstract:
In the present study, ZnO nanostructure has been synthesized by different methods, namely coprecipitation, hydrothermal and sonochemical methods. After comparison of the morphology and photocatalytic activity of ZnO samples prepared via different methods, the best method (sonochemical method) was used for synthesis of Ni-ZnO nanoparticles with different concentrations of nickel. Furthermore, structural and optical properties were investigated by Fourier Transform Infrared spectroscopy, UV–Vis spectroscopy, Field Emission Scanning Electron Microscopy, X-Ray Diffraction, and Photoluminescence spectroscopy methods. Morphology of nanoparticles prepared via sonochemical method were obtained small granular shape. In addition, the direct band gap has been calculated by Tauc's approach. Compared with pure ZnO, the band gap of the Ni-ZnO NPs is smaller and depends on the content of dopants. Moreover, photocatalytic activity of all samples has been investigated under UV irradiation in an aqueous medium. In addition, photocatalytic activity is improved in the presence of an appropriate amount of nickel dopant.
similar resources
Sonochemical synthesis of undoped and Co-doped ZnO nanostructures and investigation of optical and photocatalytic properties
In this paper, undopedZnO and Co-ZnOnano structureswith different molar ratio of Cobalt have been synthesized by the sonochemical method. Structure have been characterized by Fourier Transform (FTIR) and UV–Vis spectroscopy,Scanning Electron Microscopy (SEM), Energy Dispersive Analytical X-Ray (EDAX), and X-Ray Diffraction (XRD) methods. Moreover, the direct band gap has been calculated by Tauc...
full textSonochemical synthesis of undoped and Co-doped ZnO nanostructures and investigation of optical and photocatalytic properties
In this paper, undopedZnO and Co-ZnOnano structureswith different molar ratio of Cobalt have been synthesized by the sonochemical method. Structure have been characterized by Fourier Transform (FTIR) and UV–Vis spectroscopy,Scanning Electron Microscopy (SEM), Energy Dispersive Analytical X-Ray (EDAX), and X-Ray Diffraction (XRD) methods. Moreover, the direct band gap has been calculated by Tauc...
full textA Low Temperature Hydrothermal Synthesis of ZnO Doped SnO2 Nanoparticles with High Photocatalytic Activity
The paper reports the preparation and photocatalytic activity of ZnO doped SnO2 nanoparticles. These nanoparticles were synthesized by hydrothermal method. The products were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). Their grain sizes are about 50-100 nm. The characterization results revealed that the synthesized nanoparticles possess just cr...
full textsonochemical synthesis of undoped and co-doped zno nanostructures and investigation of optical and photocatalytic properties
in this paper, undopedzno and co-znonano structureswith different molar ratio of cobalt have been synthesized by the sonochemical method. structure have been characterized by fourier transform (ftir) and uv–vis spectroscopy,scanning electron microscopy (sem), energy dispersive analytical x-ray (edax), and x-ray diffraction (xrd) methods. moreover, the direct band gap has been calculated by tauc...
full textSonochemical Green Method for Preparation of Mg-Doped ZnO Nanostructures in Water with Enhanced Photocatalytic Activity
In this work, Mg-doped ZnO nanostructures were prepared in water under ultrasonic irradiation for 60 min without using any organic compounds or post preparation treatments. The prepared samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive analysis of X-ray (EDX), diffuse reflectance spectroscopy (DRS...
full textSynthesis and Characterization of Ni Doped ZnO Nanoparticles
This paper discerns key ideas and themes of the possibility of growing Ni doped ZnO nanoparticles by electrochemical method. The purpose is to study the growth mechanism and to optimize the parameters of this method. Upon successful synthesizing the samples, they were characterized using various techniques. XRD, SEM, FTIR, photoluminescence spectroscopy together with the measured optical parame...
full textMy Resources
Journal title
volume 6 issue 3
pages 190- 198
publication date 2016-07-01
By following a journal you will be notified via email when a new issue of this journal is published.
Hosted on Doprax cloud platform doprax.com
copyright © 2015-2023