N-(3-Chloro­phen­yl)-2,4-dimethyl­benzene­sulfonamide

نویسندگان

  • K. Shakuntala
  • Sabine Foro
  • B. Thimme Gowda
چکیده

In the mol-ecule of the title compound, C(14)H(14)ClNO(2)S, the N-H bond is in a syn position with respect to the meta-Cl atom in the aniline ring. The mol-ecule is twisted about the N-S bond with a C-SO(2)-NH-C torsion angle of 44.55 (17)°. The two aromatic rings are inclined relative to each other by 66.2 (1)°. In the crystal, N-H⋯O hydrogen bonds link the mol-ecules into infinite chains parallel to the b axis.

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منابع مشابه

N-(4-Chloro­phen­yl)-2,4-dimethyl­benzene­sulfonamide

Mol-ecules of the title compound, C(14)H(14)ClNO(2)S, are bent at the S atom with a C-SO(2)-NH-C torsion angle of 57.7 (2)°. The benzene rings are rotated relative to each other by 68.1 (1)°. In the crystal, N-H⋯O(S) hydrogen bonds pack the mol-ecules into infinite chains parallel to the b axis.

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N-(2-Chloro­phen­yl)-2,4-dimethyl­benzene­sulfonamide

In the title compound, C(14)H(14)ClNO(2)S, the conformation of the N-C bond in the C-SO(2)-NH-C segment has gauche torsions with respect to the S=O bonds. The mol-ecule is bent at the S atom with a C-SO(2)-NH-C torsion angle of -54.9 (2)°. The sulfonyl and aniline benzene rings are rotated relative to each other by 75.7 (1)°. An intra-molecular N-H⋯Cl hydrogen bond is present. In the crystal, i...

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N-(2,4-Dichloro­phen­yl)-2,4-dimethyl­benzene­sulfonamide

In the title compound, C(14)H(13)Cl(2)NO(2)S, the mol-ecule is bent at the S atom with an C-SO(2)-NH-C torsion angle of -69.9 (2)°. The dihedral angle between the sulfonyl and aniline benzene rings is 44.0 (1)°. The crystal structure features inversion dimers linked by pairs of N-H⋯O hydrogen bonds. An intra-molecular N-H⋯Cl hydrogen bond is also observed.

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N-(2,4-Dimethyl­phen­yl)-2,4-dimethyl­benzene­sulfonamide

In the crystal structure of the title compound, C(16)H(19)NO(2)S, the mol-ecule is bent at the S atom with a C-SO(2)-NH-C torsion angle of 66.5 (2)°. The dihedral angle between the sulfonyl and aniline benzene rings in the mol-ecule is 41.0 (1)°. The crystal structure features inversion dimers linked by pairs of N-H⋯O hydrogen bonds.

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عنوان ژورنال:

دوره 67  شماره 

صفحات  -

تاریخ انتشار 2011