(E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-N-(3-methoxy­phen­yl)-2,2-dimethyl­cyclo­propane­carboxamide

نویسندگان

  • Fan-Yong Yan
  • Dong-Qing Liu
چکیده

The title compound, C(16)H(17)ClF(3)NO(2), was synthesized from 3-[(E)-2-chloro-3,3,3-trifluoro-prop-1-en-yl]-2,2-dimethyl-cyclo-propane-carboxylic acid and 3-methoxy-benzenamine. The propenyl and carboxamide substituents lie on the same side of the cyclo-propane ring plane, with the two methyl substituents on either side of the plane. The benzene ring makes a dihedral angle of 76.4 (3)° with the plane of the cyclo-propane ring. The crystal structure involves intermolecular N-H⋯O hydrogen bonds.

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منابع مشابه

(E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N,N-diphenyl­cyclo­propane­carboxamide

The title compound, C(21)H(19)ClF(3)NO, was synthesized from 3-[(E)-2-chloro-3,3,3-trifluoro-prop-1-en-yl]-2,2-dimethyl-cyclo-propane-carboxylic acid and diphenyl-amine. The propenyl and carboxamide substituents lie on the same side of the cyclo-propane ring plane, with the two methyl substituents on either side of the plane. The phenyl rings of the carboxamide are inclined at an angle of 84.6 ...

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(E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N-(2-naphth­yl)cyclo­propane­carboxamide

The title compound, C(19)H(17)ClF(3)NO, was synthesized from 3-[(E)-2-chloro-3,3,3-trifluoro-prop-1-en-yl]-2,2-dimethyl-cyclopropane-carboxylic acid and 2-aminona-phthalene. There are two molecules in the asymmetric unit. The dihedral angle between the naphthalene and cyclo-propane units is 111.6 (5)°. Molecules are connected into chains by intermol-ecular N-H⋯O hydrogen bonds. One of the Cl at...

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1-{[3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl­cyclo­propan-1-yl]carbon­yl}-3-(methyl­sulfon­yl)imidazolidin-2-one

In the title mol-ecule, C(13)H(16)ClF(3)N(2)O(4)S, the imidazolidine ring is approximately planar, the largest deviation from this plane being 0.025 (3) Å. The cyclo-propane ring forms a dihedral angle of 64.1 (2)° with the imidazolidine ring. In the crystal, C-H⋯O hydrogen bonds are observed.

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(E)-3-(2-Chloro-3,3,3-trifluoro­prop-1-en­yl)-2,2-dimethyl-N-p-tolyl­cyclo­propane­carboxamide

There are two mol-ecules in the asymmetric unit of the title compound, C(16)H(17)ClF(3)NO. The benzene ring in each mol-ecule makes a dihedral angle of 66.6 (3)° [116.3 (4)° in the second mol-ecule] with the plane of the cyclo-propane ring. The F atoms of the CF(3) groups are disordered equally over two positions. The amide hydrogen is linked with the amide oxygen in another mol-ecule by an int...

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عنوان ژورنال:

دوره 64  شماره 

صفحات  -

تاریخ انتشار 2007