Rapid and Reliable Routine Analysis of Urine by Octopole Reaction Cell ICP-MS Application
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چکیده
The Agilent 7500c Inductively Coupled Plasma Mass Spectrometer (ICP-MS) was used for the fast, routine, and reliable analysis of 23 trace elements in urine. The complete method validation for all elements is described, including the evaluation of short-term and long-term stability, the analysis of different reference materials and the discussion of precision and accuracy in internal and external quality assurance. The urine samples were analyzed directly after a low dilution of 1/5 (v/v) with 1% (v/v) nitric acid. Using this simple sample preparation method, one operator can prepare more than 100 samples in less than 1 hour. An ICP-MS fitted with an octopolebased collision/reaction cell enables the simultaneous determination of all 23 elements either in the normal concentration range for the essential elements or at concentration levels relevant for occupational and environmental health. Rapid and Reliable Routine Analysis of Urine by Octopole Reaction Cell ICP-MS Application
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Rapid and Reliable Routine Analysis of Urine by Octopole Reaction Cell ICP-MS Application
The Agilent 7500c Inductively Coupled Plasma Mass Spectrometer (ICP-MS) was used for the fast, routine, and reliable analysis of 23 trace elements in urine. The complete method validation for all elements is described, including the evaluation of short-term and long-term stability, the analysis of different reference materials and the discussion of precision and accuracy in internal and externa...
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