N′-(2,4-Dichloro­benzyl­idene)-4-methoxy­benzohydrazide methanol solvate

نویسندگان

  • Min Liang
  • Dong-Hui Zou
چکیده

In the title compound, C(15)H(12)Cl(2)N(2)O(2)·CH(3)OH, the hydrazone mol-ecule displays an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 4.6 (2)°. In the crystal structure, the hydrazone and methanol mol-ecules are linked into a chain propagating along the a axis via N-H⋯O and O-H⋯O hydrogen bonds.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

N′-(2,4-Dichloro­benzyl­idene)-3-methoxy­benzohydrazide

There are two independent mol-ecules in the asymmetric unit of the title compound, C(15)H(12)Cl(2)N(2)O(2). The dihedral angle between the two benzene rings is 27.6 (4)° in one mol-ecule and 16.4 (4)° in the other. Both mol-ecules adopt an E configuration about the C=N bonds. In the crystal structure, mol-ecules are linked through inter-molecular N-H⋯O hydrogen bonds, forming chains in the a-ax...

متن کامل

N′-(3,5-Dichloro-2-hydroxy­benzyl­idene)-3-methoxy­benzohydrazide methanol solvate

In the title compound, C(15)H(12)Cl(2)N(2)O(3)·CH(3)OH, the Schiff base mol-ecule is nearly planar, with a dihedral angle of 4.5 (2)° between the two benzene rings. An intra-molecular O-H⋯N hydrogen bond is observed. The methanol solvent mol-ecule is linked to the Schiff base mol-ecule through inter-molecular N-H⋯O and O-H⋯O hydrogen bonds.

متن کامل

2,4-Dichloro-6-(8-quinolylamino­methyl­ene)cyclo­hexa-2,4-dien-1-one methanol solvate

The main mol-ecule of the title methanol solvate, C(16)H(10)Cl(2)N(2)O·CH(3)OH, exists in the keto form and the C=O and N-H bonds are mutually cis in the crystal structure. The dihedral angle between the quinoline and benzene rings is 11.17 (3)°. A bifurcated intra-molecular N-H⋯(O,N) hydrogen bond is present as well as an O-H⋯O hydrogen bond. In the crystal, C-H⋯O inter-actions link the 3,5-di...

متن کامل

(E)-3-Bromo-N′-(2,4-dichloro­benzyl­idene)benzohydrazide

The title compound, C(14)H(9)BrCl(2)N(2)O, was synthesized by the reaction of 2,4-dichloro-benzaldehyde with an equimolar quantity of 3-bromo-benzohydrazide in methanol. The mol-ecule displays an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 5.3 (2)°. In the crystal structure, mol-ecules are linked through inter-molecular N-H⋯O and C-H⋯O hydrogen bonds,...

متن کامل

(Z)-2-Amino-5-[2,4-dimeth­oxy-6-(4-methoxy­styr­yl)benzyl­idene]-1,3-thia­zol-4(5H)-one methanol solvate

In the crystal structure of the title compound, C(21)H(20)N(2)O(4)S·CH(3)OH, mol-ecules are linked into chains by a series of inter-molecular N-H⋯O, N-H⋯N and O-H⋯O hydrogen bonds. The mol-ecular structure shows a double bond with Z geometry, connecting the thia-zolone and resveratrol units. The dihedral angle between the thiazolone ring and the nearest dimethoxy-benzene ring is 53.02 (7)°.

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره 65  شماره 

صفحات  -

تاریخ انتشار 2009