Crystal structure of 2,8,14-trimethyl-2,8,14-triazatetracyclo- [14(2,24),7,2(10,13)]tetracosa-4,6,10,12,16,18,19,21,23-nonaene-3,9,15-trione.

نویسندگان

  • I Azumaya
  • T Okamoto
  • H Takayanagi
چکیده

both as crystals and in solution.1–3 A cyclic structure containing N-methylamide can be easily constructed, since the cis preference arranges two moieties attached to the N-methylated amide close to each other. In this paper, we report on the crystal structure of 2,8,14-trimethyl-2,8,14-triazatetracyclo[142,24,7,210,13]tetracosa-4,6,10,12,16,18,19,21,23-nonaene3,9,15-trione (1, Fig. 1), which was synthesized by a one-pot reaction (43% yield) from 4-(methylamino)benzoic acid under 1363 ANALYTICAL SCIENCES NOVEMBER 2001, VOL. 17 2001 © The Japan Society for Analytical Chemistry

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عنوان ژورنال:
  • Analytical sciences : the international journal of the Japan Society for Analytical Chemistry

دوره 17 11  شماره 

صفحات  -

تاریخ انتشار 2001