High-throughput x-ray characterization system for combinatorial materials studies

نویسندگان

  • Zhenlin Luo
  • Bin Geng
  • Jun Bao
  • Cihui Liu
  • Wenhan Liu
  • Chen Gao
  • Zhiguo Liu
  • Xunliang Ding
چکیده

We have developed a high-throughput x-ray characterization system, which can rapidly screen structure, composition and x-ray scintillation of combinatorial materials libraries using energy-dispersive x-ray diffraction, x-ray fluorescence, and x-ray photoluminescence. This system consists of an x-ray source, a polycapillary x-ray lens, one or two x-ray energy detectors, and a fiber optic spectrometer. A Windows-based software package was also developed to control the measurement system and data acquisition automatically. Examples are also demonstrated to show the applicability of this system. © 2005 American Institute of Physics. DOI: 10.1063/1.2038147

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

High-throughput synchrotron X-ray diffraction for combinatorial phase mapping.

Discovery of new materials drives the deployment of new technologies. Complex technological requirements demand precisely tailored material functionalities, and materials scientists are driven to search for these new materials in compositionally complex and often non-equilibrium spaces containing three, four or more elements. The phase behavior of these high-order composition spaces is mostly u...

متن کامل

High-throughput determination of structural phase diagram and constituent phases using GRENDEL.

Advances in high-throughput materials fabrication and characterization techniques have resulted in faster rates of data collection and rapidly growing volumes of experimental data. To convert this mass of information into actionable knowledge of material process-structure-property relationships requires high-throughput data analysis techniques. This work explores the use of the Graph-based endm...

متن کامل

High Throughput Light Absorber Discovery, Part 2: Establishing Structure-Band Gap Energy Relationships.

Combinatorial materials science strategies have accelerated materials development in a variety of fields, and we extend these strategies to enable structure-property mapping for light absorber materials, particularly in high order composition spaces. High throughput optical spectroscopy and synchrotron X-ray diffraction are combined to identify the optical properties of Bi-V-Fe oxides, leading ...

متن کامل

Parallel solution combustion synthesis for combinatorial materials studies.

A parallel solution combustion synthesis technique was developed for combinatorial materials studies. The vigorous combustion reactions were successfully limited in the microreactors by using a substrate-net-mask microreactor system and the lowest adoptable furnace temperature. Using this technique, a luminescent materials library of Y3Al5O12/Tb(chi) was synthesized with the aid of an ink-jet d...

متن کامل

Elements of informatics for combinatorial solid - state materials science

The main purpose of using combinatorial techniques for materials science studies is to achieve higher experimental throughput than what is possible when samples are synthesized and characterized one at a time. The instrumentation needed for performing high-throughput synthesis and characterization has seen rapid development in recent years. The software tools needed to connect all parts of the ...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 2005