Cost-effective upgrade of a focusing system for inelastic X-ray scattering experiments under high pressure

نویسندگان

  • Chi-Yi Huang
  • Yong Q. Cai
  • Nozomu Hiraoka
  • Cheng-Chi Chen
  • Shih-Chun Chung
  • Yen-Fang Song
  • King-Long Tsang
چکیده

Inelastic X-ray scattering (IXS) is a powerful technique capable of probing the dynamic behavior and electronic structure of materials. For IXS experiments under high pressure up to the megabar range using state-of-the-art diamond-anvil-cell technology, the sample volume is limited to the order of 1 x 10(-3) mm(3) for which a beam focus of the same order and less is often required. In this paper a scheme utilizing a set of low-cost and compact Kirkpatrick-Baez mirrors for upgrading the existing optical system of the Taiwan IXS beamline at SPring-8 is described. The scheme as implemented improves the focus to 13 microm x 16 microm (horizontal x vertical) with a transmission of up to 72% and a flux density gain of over 30 times, which has enhanced substantially the efficiency of the beamline for high-pressure research.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

نرم شدگی فونون‌های انرژی بالا با گذار عایق - ابررسانا در سیستم ابررسانای Ba1-xKxBiO3

Single crystals of Ba1-xKxBiO3 compound for 0 < x <0.6 from insulator to superconducting region have been grown by electrochemical method. The crystals have been characterized by powder x-ray diffraction and Laue x-ray to determine the crystal structure, formed phases and potassium concentration. Inelastic x-ray scattering spectrum of the crystals has been studied to investigate the phonon pro...

متن کامل

Focusing polycapillary to reduce parasitic scattering for inelastic x-ray measurements at high pressure.

The double-differential scattering cross-section for the inelastic scattering of x-ray photons from electrons is typically orders of magnitude smaller than that of elastic scattering. With samples 10-100 μm size in a diamond anvil cell at high pressure, the inelastic x-ray scattering signals from samples are obscured by scattering from the cell gasket and diamonds. One major experimental challe...

متن کامل

Amorphous boron gasket in diamond anvil cell research

Recent advances in high-pressure diamond anvil cell experiments include high-energy synchrotron x-ray techniques as well as new cell designs and gasketing procedures. The success of high-pressure experiments usually depends on a well-prepared sample, in which the gasket plays an important role. Various gasket materials such as diamond, beryllium, rhenium, and stainless steel have been used. Her...

متن کامل

Inelastic X-ray Scattering by Electronic Excitations under High Pressure

Investigating electronic structure and excitations under extreme conditions gives access to a rich variety of phenomena. High pressure typically induces behavior such as magnetic collapse and the insulator-metal transition in 3d transition metals compounds, valence fluctuations or Kondo-like characteristics in f -electron systems, and coordination and bonding changes in molecular solids and gla...

متن کامل

Inelastic X-ray Scattering by Electronic Excitations in Solids at High Pressure

Investigating electronic structure and excitations under extreme conditions gives access to a rich variety of phenomena. High pressure typically induces behavior such as magnetic collapse and the insulator-metal transition in 3d transition metals compounds, valence fluctuations or Kondo-like characteristics in f -electron systems, and coordination and bonding changes in molecular solids and gla...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:
  • Journal of Synchrotron Radiation

دوره 15  شماره 

صفحات  -

تاریخ انتشار 2008