Generating single metalloprotein crystals in well-defined redox states: electrochemical control combined with infrared imaging of a NiFe hydrogenase crystal† †Electronic supplementary information (ESI) available: Crystal preparation; cyclic voltammogram in the experimental cell; position-dependent difference spectra; demonstration of control over all active sites; visible images of a crystal recorded periodically during measurements; time-dependent Nia-R formation. See DOI: 10.1039/c7cc02591b

Polymorph crystal packing effects on charge transfer emission in the solid state† †Electronic supplementary information (ESI) available: X-ray data, temperature dependent fluorescence spectra, FLIM data, fluorescence microscope images and calculations. CCDC 1003612 and 1003613. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c5sc01151e

Synthesis and Crystal Growth of Sb2S3 Nanorods Using Iodine as an Initiator Material via Electrochemical Mechanism in Hydrothermal Condition

Crystalline antimony sulfide (Sb2S3) with nanorods morphology was successfully prepared via hydrothermal method by the reaction of elemental sulfur, antimony and iodine as starting materials with high yield at 180°C for 24h.Using oxidation reagents like iodine as an initiator of redox reaction to prepare Sb2S3 is reported for first time. Crystal growth of Sb2S3 was done by increasing reaction t...

Single crystal structures and theoretical calculations of uranium endohedral metallofullerenes (U@C 2n, 2n = 74, 82) show cage isomer dependent oxidation states for U† †Electronic supplementary information (ESI) available. CCDC 1508508 1508509 1522558. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c7sc01711a Click here for additional data file. Click here for additional data file.

Department of Chemistry, University of Texa Paso, Texas 79968, USA. E-mail: echegoyen@ Departament de Qúımica F́ısica i Inorgànic Domingo 1, 43007 Tarragona, Spain Laboratory of Advanced Optoelectronic Ma Engineering and Materials Science, Soochow R. China † Electronic supplementary information ( 1522558. For ESI and crystallographic dat DOI: 10.1039/c7sc01711a Cite this: Chem. Sci., 2017, 8, 5282

Anion exchange coupled with the reduction and dimerisation of a copper(ii) nitrate complex of tripyridyl dithioether via a single-crystal-to-single-crystal transformation† †Electronic supplementary information (ESI) available: PXRD patterns, ESI-MS spectrum, SEM images, AFM images, UV spectra, crystal structures and TGA data. CCDC 1511571–1511577. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c6sc05341f Click here for additional data file. Click here for additional data file.

Department of Chemistry, Research Institute University, Jinju 52828, South Korea. E-ma Tel: +82 55-772-1483 Education Center, Faculty of Engineering Shibazono, Narashino, Chiba 275-0023, Jap Department of Chemistry, Toho University 8510, Japan † Electronic supplementary information spectrum, SEM images, AFM images, U data. CCDC 1511571–1511577. For ESI an electronic format see DOI: 10.1039/c6sc...

Crystalline boron-linked tetraaminoethylene radical cations† †Electronic supplementary information (ESI) available: NMR spectra, crystallographic data, crystal structures, UV-vis spectra, cyclic voltammograms, EPR spectra, and theoretical calculation. CCDC 1548460–1548466. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c7sc03528d Click here for additional data file. Click here for additional data file.