Preparation and Purification of Hydrogen Deuteride
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چکیده
In an investigation of t he physical properties of hydr<;>gen isotopes it was n.ecessar.\:' t o prepare 10 liters of high-purity. hydro~en d~u.tende. TI1JS was don e ~y r eactmg IJ t hlUm aluminum hydride wit h deutenum oXIde, gly.;n~ hydro~en deutende, ]I) .t wo batch~s, ?f 98.1and 97.0-percent purity, respect ive!.\:' . .Ihls mater!ai was t hen frac t IOnated at JtqUJd hydrogen t emperature in t hree batches, Yleldmg the desIred amoun t of hydrogen deutende in a puri ty of 99.8 percent.
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تاریخ انتشار 2011