atomic absorption spectrometric determination of lead after extraction and preconcentration with 5-br-padap
نویسندگان
چکیده
lead is quantitatively retained on 2-(5-bromo-2-pyridylazo)-5-diethylaminophenol (5-br-padap)-ammonium tetraphenylborate with microcrystalline naphthalene or by a column method in the ph range 4.0-6.0 from a large volume of aqueous solutions of various samples with preconcentration factor of 60. after filtration, the solid mass consisting of the lead complex and naphthalene was dissolved with 5 ml of dimethylformamide and the metal was determined by atomic absorption spectrometry. the calibration curve is linear in the range of 1.9-180 mg/ml in dmf with a relative standard deviation 1.7&. the interference of a large number of anions and cations has been studied.
منابع مشابه
Atomic Absorption Spectrometric Determination of Lead after Extraction and Preconcentration with 5-Br-PADAP
Lead is quantitatively retained on 2-(5-bromo-2-pyridylazo)-5-diethylaminophenol (5-Br-PADAP)-ammonium tetraphenylborate with microcrystalline naphthalene or by a column method in the pH range 4.0-6.0 from a large volume of aqueous solutions of various samples with preconcentration factor of 60. After filtration, the solid mass consisting of the lead complex and naphthalene was dissolved wi...
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عنوان ژورنال:
iranian journal of chemistry and chemical engineering (ijcce)ناشر: iranian institute of research and development in chemical industries (irdci)-acecr
ISSN 1021-9986
دوره 20
شماره 1 2001
میزبانی شده توسط پلتفرم ابری doprax.com
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