Synthesis of Tri-substituted Thiopseudoureas and its Desulfurization

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Synthesis of 1,3,5-tri-substituted pyrazoles promoted by P2O5.SiO2

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synthesis of 1,3,5-tri-substituted pyrazoles promoted by p2o5.sio2

silica supported phosphorus pentoxide (p2o5·sio2) is an efficient catalyst for synthesis of 1,3,5-substituted pyrazoles via the condensation of 1,3-diketones and hydrazines. simplicity of procedure, mild condition, being solvent-free, high yields, and easy workup are some advantages of this protocol.

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ژورنال

عنوان ژورنال: YAKUGAKU ZASSHI

سال: 1964

ISSN: 0031-6903,1347-5231

DOI: 10.1248/yakushi1947.84.9_830